Energy Fuels, 21 (3), 1777 -1781, 2007. 10.1021/ef0606207 S0887-0624(06)00620-7
Web Release Date: March 15, 2007

Copyright © 2007 American Chemical Society

Continuous-Flow Preparation of Biodiesel Using Microwave Heating

T. Michael Barnard, Nicholas E. Leadbeater,* Matthew B. Boucher, Lauren M. Stencel, and Benjamin A. Wilhite

CEM Corporation, 3100 Smith Farm Road, Matthews, North Carolina 28106, and UCONN Biofuels Consortium, University of Connecticut, Storrs, Connecticut 06269-3060

Received December 6, 2006

Revised Manuscript Received February 1, 2007

Abstract:

The continuous-flow preparation of biodiesel using a commercially available scientific microwave apparatus offers a fast, easy route to this valuable biofuel. The methodology allows for the reaction to be run under atmospheric conditions and performed at flow rates of up to 7.2 L/min using a 4 L reaction vessel. It can be utilized with new or used vegetable oil with methanol and a 1:6 molar ratio of oil/alcohol. Energy consumption calculations suggest that the continuous-flow microwave methodology for the transesterification reaction is more energy-efficient than using a conventional heated apparatus.


Download the full text: PDF | HTML