Web Release Date: March 15,
Continuous-Flow Preparation of Biodiesel Using Microwave Heating


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CEM Corporation, 3100 Smith Farm Road, Matthews, North Carolina 28106, and UCONN Biofuels Consortium, University of Connecticut, Storrs, Connecticut 06269-3060
Received December 6, 2006
Revised Manuscript Received February 1, 2007
Abstract:
The continuous-flow preparation of biodiesel using a commercially available scientific microwave apparatus offers a fast, easy route to this valuable biofuel. The methodology allows for the reaction to be run under atmospheric conditions and performed at flow rates of up to 7.2 L/min using a 4 L reaction vessel. It can be utilized with new or used vegetable oil with methanol and a 1:6 molar ratio of oil/alcohol. Energy consumption calculations suggest that the continuous-flow microwave methodology for the transesterification reaction is more energy-efficient than using a conventional heated apparatus.
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