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1H NMR, 13C NMR, and Mass Spectrometry of 1-Phenyl-1,2-Dihaloethanes

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Joseph R. Gandler , Kevin W. Kittredge and Oliver L. Saunders

California State University, Fresno, CA 93740

J. Chem. Educ., 1995, 72 (9), p 855

DOI: 10.1021/ed072p855

Publication Date: September 1995

Abstract

¹H NMR, ¹³C NMR, and mass spectra are reported for a series of 1-phenyl-1,2-dihaloethanes. These spectra have been utilized in introductory organic chemistry to illustrate the complementary nature of these spectroscopic methods in characterizing molecular structure, and as a means of introducing students to ¹³C NMR chemical shift calculations.

Keywords (Audience):

Second-Year Undergraduate

Keywords (Domain):

Organic Chemistry

Keywords (Pedagogy):

Hands-On Learning / Manipulatives

Keywords (Subject):

NMR Spectroscopy

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This article has been cited by 1 ACS Journal articles (1 most recent appear below).

Deuterium Exchange in Ethyl Acetoacetate: An Undergraduate GC–MS Experiment
C.D. Heinson , J. M. Williams , W. N. Tinnerman and T. B. Malloy
Journal of Chemical Education2005 82 (5), 787
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  C.D. Heinson , J. M. Williams , W. N. Tinnerman and T. B. Malloy
  Journal of Chemical Education2005 82 (5), 787
  A simple experiment involving deuterium exchange of the enolizable protons in ethyl acetoacetate followed by GC–MS has been developed. The principles demonstrated are the use of stable isotopes, keto–enol tautomerism, base catalysis, and the use of ...
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