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A Glycosidation Reaction Employing Montmorillonite K-10 as Catalyst

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Brooke L. Bedell , R. David Crouch , Michael S. Holden and Heidi E. Martinson

Department of Chemsitry, Dickinson College, PO Box 1773, Carlisle, PA 17013-2896

J. Chem. Educ., 1996, 73 (11), p 1041

DOI: 10.1021/ed073p1041

Publication Date (Web): November 1, 1996

Section:

History, Education, and Documentation

Abstract

The large number of biology majors and prehealth students enrolled in Organic Chemistry makes it desirable to have laboratories that involve biologically interesting molecules. Although many laboratory manuals contain sections on carbohydrate chemistry, the experiments are typically limited to esterification or hydrolysis reactions. A recent publication (Toshima, K.; Ishizuka, T.; Matsuo, G.; Nakata, M. Synlett. 1995, 306. ) on the glycosidation of glycals offered a different possibility.

Keywords (Audience):

Upper-Division Undergraduate

Keywords (Domain):

Biochemistry

Keywords (Feature):

The Microscale Laboratory

Keywords (Pedagogy):

Hands-On Learning / Manipulatives

Keywords (Subject):

Catalysis

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This article has been cited by 1 ACS Journal articles (1 most recent appear below).

Glycosidation of Methanol with Ribose: An Interdisciplinary Undergraduate Laboratory Experiment
Erin Simon, Katie Cook, Meredith R. Pritchard, Wayne Stripe, Martha Bruch and Kestutis Bendinskas
Journal of Chemical Education2010 87 (7), 739-741
- Glycosidation of Methanol with Ribose: An Interdisciplinary Undergraduate Laboratory Experiment
  Erin Simon, Katie Cook, Meredith R. Pritchard, Wayne Stripe, Martha Bruch and Kestutis Bendinskas
  Journal of Chemical Education2010 87 (7), 739-741
  This exercise provides students hands-on experience with the topics of glycosidation, hemiacetal and acetal formation, proton nuclear magnetic resonance (1H NMR) spectroscopy, and kinetic and thermodynamic product formation. In this laboratory experiment, ...
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