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Inexpensive Small-Scale Sonochemistry with Magnetic Agitation
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Abstract
A reduction, esterification, acetylation, an ether synthesis, and an aryl nucleophilic substitution are performed in a microwave oven.
Keywords (Audience):
First-Year Undergraduate / GeneralKeywords (Feature):
The Microscale LaboratoryKeywords (Subject):
Microscale LabCiting Articles
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This article has been cited by 9 ACS Journal articles (5 most recent appear below).
Microwave-Enhanced Organic Syntheses for the Undergraduate Laboratory: Diels−Alder Cycloaddition, Wittig Reaction, and Williamson Ether Synthesis
Marsha R. Baar, Danielle Falcone and Christopher GordonJournal of Chemical Education2010 87 (1), 84-86Microwave-Enhanced Organic Syntheses for the Undergraduate Laboratory: Diels−Alder Cycloaddition, Wittig Reaction, and Williamson Ether Synthesis
Marsha R. Baar, Danielle Falcone and Christopher GordonJournal of Chemical Education2010 87 (1), 84-86Microwave heating enhanced the rate of three reactions typically performed in our undergraduate organic chemistry laboratory: a Diels−Alder cycloaddition, a Wittig salt formation, and a Williamson ether synthesis. Ninety-minute refluxes were shortened to ...
The State of Organic Teaching Laboratories
Gail HorowitzJournal of Chemical Education2007 84 (2), 346The State of Organic Teaching Laboratories
Gail HorowitzJournal of Chemical Education2007 84 (2), 346This review explores the dramatic changes that have taken place in the organic chemistry laboratory course over the last two to three decades. The most significant changes have been in the areas of pedagogy and technology. Significant inroads have been ...
Microwave-Mediated Synthesis of Lophine: Developing a Mechanism To Explain a Product
R. David Crouch , Jessica L. Howard , Jennifer L. Zile and Kathryn H. BarkerJournal of Chemical Education2006 83 (11), 1658Microwave-Mediated Synthesis of Lophine: Developing a Mechanism To Explain a Product
R. David Crouch , Jessica L. Howard , Jennifer L. Zile and Kathryn H. BarkerJournal of Chemical Education2006 83 (11), 1658The microwave-mediated preparation of lophine (2,4,5-triphenylimidazole) is described. This experiment allows for an introduction to the emerging technology of microwave-assisted organic synthesis while providing an opportunity for students to employ the ...
Incorporation of Microwave Synthesis into the Undergraduate Organic Laboratory
E. Keller Barnhardt , Alan R. Katritzky , Chunming Cai , Meghan D. Collins , Eric F. V. Scriven and Sandeep K. SinghJournal of Chemical Education2006 83 (4), 634Incorporation of Microwave Synthesis into the Undergraduate Organic Laboratory
E. Keller Barnhardt , Alan R. Katritzky , Chunming Cai , Meghan D. Collins , Eric F. V. Scriven and Sandeep K. SinghJournal of Chemical Education2006 83 (4), 634As the acceptance of microwave synthesis grows, it becomes increasingly important for undergraduate chemists to fully learn about this emerging technology. Advances have made microwave use in the undergraduate laboratory safe, easy, and affordable. Herein ...
Microwave-Assisted Heterocyclic Chemistry for Undergraduate Organic Laboratory
Robert Musiol , Bozena Tyman-Szram and Jaroslaw PolanskiJournal of Chemical Education2006 83 (4), 632Microwave-Assisted Heterocyclic Chemistry for Undergraduate Organic Laboratory
Robert Musiol , Bozena Tyman-Szram and Jaroslaw PolanskiJournal of Chemical Education2006 83 (4), 632Heterocyclic chemistry forms an interesting and important part of organic chemistry. Microwave-assisted techniques were applied to design new environmentally benign syntheses of heterocycles for the undergraduate organic laboratory. To avoid toxic ...
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- Received: August 03, 2009
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