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The Synthesis of 10-[Spiro[6,6]C60]-Anthrone: A Microscale Reaction of Fullerene
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Abstract
The microscale 1,3-dipolar cycloaddition reaction of Fullerene-C60 with 10-diazoanthrone leading to the methanofullerene adduct is described. The synthesis of the monoadduct and flash chromatography separation of the formed bisadducts was set up for two three hour laboratory periods.
Keywords (Domain):
Laboratory InstructionKeywords (Feature):
The Microscale LaboratoryKeywords (Pedagogy):
Hands-On Learning / ManipulativesKeywords (Subject):
SynthesisCiting Articles
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This article has been cited by 1 ACS Journal articles (1 most recent appear below).
Derivatization of Fullerenes: An Organic Chemistry Laboratory
Charles T. Cox and Melanie M. CooperJournal of Chemical Education2006 83 (1), 99Derivatization of Fullerenes: An Organic Chemistry Laboratory
Charles T. Cox and Melanie M. CooperJournal of Chemical Education2006 83 (1), 99Fullerene chemistry is a rapidly expanding research field that has grown immensely over the past decade. However, little fullerene chemistry is being incorporated into undergraduate lectures or laboratories, and there have only been two contributions in ...
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- Received: August 03, 2009
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