Getting Close with the Instructional Scanning Tunneling Microscope

Carl Steven Rapp
East Tennessee State University, University School, Box 70632, Johnson City, TN 37614
J. Chem. Educ., 1997, 74 (9), p 1087
DOI: 10.1021/ed074p1087
Publication Date (Web): September 1, 1997

Abstract

Scanning Tunneling Electron Microscopy (STEM) is a powerful technique that provides magnification of conducting surfaces to the atomic level. My recent experience as a member of a group of twenty teachers selected to work for eight summer weeks with scientists at Xerox Corporation and professors at the University of Rochester has opened new vistas for me and my high school students. We learned to use the Burleigh Instructional Scanning Tunneling Microscope (ISTM), an instrument designed for educational use by the University of Rochester, Xerox Corporation, and Burleigh Instrument Inc. While the images we can produce are not of the same quality as are often seen in the research literature, care in making a sharp, uncontaminated scanning tip and data collection in a vibration-free area, can result in pictures that are more than adequate for the introduction of "atomic eyes" to my classroom.

The ISTM is useful in the study of the effect of acids and bases on metals and the surfaces of semiconductors (some experiments are described below). Cutting the platinum-iridium tip or preparing the tungsten tip and mounting the sample are hands-on activities that give students a glimpse of the technological nanoworld. This state-of-the-art instrumentation is making it possible for students to actually view atoms in their own classroom. What is truly amazing, however, is that the ISTM can be set up and atomic resolution images obtained in about an hour.

Keywords (Audience):

High School / Introductory Chemistry

Keywords (Feature):

Secondary School Chemistry

Keywords (Pedagogy):

Computer-Based Learning

Keywords (Subject):

Instrumental Methods

Citing Articles

Citation data is made available by participants in CrossRef's Cited-by Linking service. For a more comprehensive list of citations to this article, users are encouraged to perform a search in SciFinder.

This article has been cited by 12 ACS Journal articles (5 most recent appear below).

  • Cover Image

    Exploring the Scanning Probe: A Simple Hands-on Experiment Simulating the Operation and Characteristics of the Atomic Force Microscope

    Anthony Layson, Ryan Leib and Dale Teeters
    2010 1010 (), 167-176
    • Exploring the Scanning Probe: A Simple Hands-on Experiment Simulating the Operation and Characteristics of the Atomic Force Microscope

      Anthony Layson, Ryan Leib and Dale Teeters
      2010 1010 (), 167-176

      A simple yet effective model atomic force microscope is presented for the purpose of introducing students to the field of scanning probe microscopy. The model is used to demonstrate the basic characteristics of the atomic force microscope by realistically ...

  • Cover Image

    "We Actually Saw Atoms with Our Own Eyes". Conceptions and Convictions in Using the Scanning Tunneling Microscope in Junior High School

    Hannah Margel , Bat-Sheva Eylon and Zahava Scherz
    Journal of Chemical Education2004 81 (4), 558
    • "We Actually Saw Atoms with Our Own Eyes". Conceptions and Convictions in Using the Scanning Tunneling Microscope in Junior High School

      Hannah Margel , Bat-Sheva Eylon and Zahava Scherz
      Journal of Chemical Education2004 81 (4), 558

      A new avenue of teaching the structure of materials is possible as a result of the development of high-resolution microscopes such as the scanning tunneling microscope (STM), which enables inspection of materials at atomic-level resolution. The purpose of ...

  • Cover Image

    Investigating Intermolecular Interactions via Scanning Tunneling Microscopy. An Experiment for the Physical Chemistry Laboratory

    David Pullman and Karen I. Peterson
    Journal of Chemical Education2004 81 (4), 549
    • Investigating Intermolecular Interactions via Scanning Tunneling Microscopy. An Experiment for the Physical Chemistry Laboratory

      David Pullman and Karen I. Peterson
      Journal of Chemical Education2004 81 (4), 549

      A laboratory experiment is presented that uses a scanning tunneling microscope to probe intermolecular interactions. In the first part of the project, the students produce and analyze images of graphite and use these images to calibrate the scan size of ...

  • Cover Image

    Atomic Scale Imaging: A Hands-On Scanning Probe Microscopy Laboratory for Undergraduates

    Chuan-Jian Zhong , Li Han , Mathew M. Maye , Jin Luo , Nancy N. Kariuki and Wayne E. Jones Jr.
    Journal of Chemical Education2003 80 (2), 194
    • Atomic Scale Imaging: A Hands-On Scanning Probe Microscopy Laboratory for Undergraduates

      Chuan-Jian Zhong , Li Han , Mathew M. Maye , Jin Luo , Nancy N. Kariuki and Wayne E. Jones Jr.
      Journal of Chemical Education2003 80 (2), 194

      A new hands-on laboratory experiment using a scanning probe microscope is described for an advanced undergraduate course. The laboratory involves a combination of scanning tunneling microscopy (STM) and atomic force microscopy (AFM) with an emphasis on ...

  • Cover Image

    Visualizing Atoms, Molecules and Surfaces by Scanning Probe Microscopy

    Kimberly Aumann , Karen J. C. Muyskens and Kumar Sinniah
    Journal of Chemical Education2003 80 (2), 187
    • Visualizing Atoms, Molecules and Surfaces by Scanning Probe Microscopy

      Kimberly Aumann , Karen J. C. Muyskens and Kumar Sinniah
      Journal of Chemical Education2003 80 (2), 187

      In this paper we describe several examples of scanning probe microscopy (SPM) experiments that we have carried out during a three-week undergraduate introductory course during our January interim term and as independent undergraduate research projects. ...

Tools

SciFinder Links

SciFinder subscribers:  Click to sign in | Not a SciFinder subscriber? Learn more at www.cas.org

Explore by:


History

  • Received: August 03, 2009

Recommend & Share

  • Share on ACS NetworkACS Network
  • Add to FacebookFacebook
  • Tweet ThisTweet This
  • Add to CiteULikeCiteULike
  • Add to NewsvineNewsvine
  • Digg ThisDigg This
  • Add to DeliciousDelicious

Related Content

See also: