Microscale Synthesis and 1H NMR Analysis of Tetraphenylporphyrins

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Abstract

Citing Articles

View all 9 citing articles

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This article has been cited by 9 ACS Journal articles (5 most recent appear below).

• 

  Accurate Specification of Molecular Structures: The Case for Zero-Order Bonds and Explicit Hydrogen Counting

  Alex M. Clark
  Journal of Chemical Information and Modeling2011 51 (12), 3149-3157

  • Accurate Specification of Molecular Structures: The Case for Zero-Order Bonds and Explicit Hydrogen Counting

    Alex M. Clark
    Journal of Chemical Information and Modeling2011 51 (12), 3149-3157

    Most data structures used to represent molecular entities for cheminformatics are underspecified for purposes of representing nonorganic chemical species. Two extensions are proposed: allowing bond orders of 0 and adding an atom property to control the ...

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• 

  Egg-Citing! Isolation of Protoporphyrin IX from Brown Eggshells and Its Detection by Optical Spectroscopy and Chemiluminescence

  Michelle L. Dean, Tyson A. Miller, and Christian Brückner
  Journal of Chemical Education2011 88 (6), 788-792

  • Egg-Citing! Isolation of Protoporphyrin IX from Brown Eggshells and Its Detection by Optical Spectroscopy and Chemiluminescence

    Michelle L. Dean, Tyson A. Miller, and Christian Brückner
    Journal of Chemical Education2011 88 (6), 788-792

    A simple and cost-effective laboratory experiment is described that extracts protoporphyrin IX from brown eggshells. The porphyrin is characterized by UV−vis and fluorescence spectroscopy. A chemiluminescence reaction (peroxyoxalate ester fragmentation) ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Iron(II)-Catalyzed Amidation of Aldehydes with Iminoiodinanes at Room Temperature and under Microwave-Assisted Conditions

  Thi My Uyen Ton, Ciputra Tejo, Stefani Tania, Joyce Wei Wei Chang, and Philip Wai Hong Chan
  The Journal of Organic Chemistry2011 Article ASAP

  • Iron(II)-Catalyzed Amidation of Aldehydes with Iminoiodinanes at Room Temperature and under Microwave-Assisted Conditions

    Thi My Uyen Ton, Ciputra Tejo, Stefani Tania, Joyce Wei Wei Chang, and Philip Wai Hong Chan
    The Journal of Organic Chemistry2011 Article ASAP

    A method for the amidation of aldehydes with PhI═NTs/PhI═NNs as the nitrogen source and an inexpensive iron(II) chloride + pyridine as the in situ formed precatalyst under mild conditions at room temperature or microwave assisted conditions is described. ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Benzoylation of Ergosterol through Nucleophilic Acyl Substitution and Subsequent Formation of Ergosterol Benzoate Endoperoxide by Reaction with Singlet Oxygen Generated by Photosensitization

  Mary C. Roslaniec, Elizabeth M. Sanford
  Journal of Chemical Education2011 88 (2), 229-231

  • Benzoylation of Ergosterol through Nucleophilic Acyl Substitution and Subsequent Formation of Ergosterol Benzoate Endoperoxide by Reaction with Singlet Oxygen Generated by Photosensitization

    Mary C. Roslaniec, Elizabeth M. Sanford
    Journal of Chemical Education2011 88 (2), 229-231

    Reactive oxygen species such as singlet oxygen have been a major focus of research in medicine. The effect of singlet oxygen on sterols within biological membranes is becoming increasingly more important. Ergosterol, a vitamin D precursor, is one such ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Microscale Synthesis and 1H NMR Analysis of ZnII and NiII Tetraphenylporphyrins

  Laura Saucedo and Larry M. Mink
  Journal of Chemical Education2005 82 (5), 790

  • Microscale Synthesis and 1H NMR Analysis of ZnII and NiII Tetraphenylporphyrins

    Laura Saucedo and Larry M. Mink
    Journal of Chemical Education2005 82 (5), 790

    A multiweek undergraduate laboratory involving the microscale synthesis of porphyrins and the corresponding metalloporphyrins is presented. All of the synthetic products are isolated as solid compounds, allowing for their analysis by UV–visible and 1H NMR ...

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