A Simple Laboratory-Constructed Automatic Titrator

Kurt L. Headrick , Terry K. Davies and Aaron N. Haegele
Department of Chemistry, University of Victoria, Victoria, BC V8W 3V6, Canada
J. Chem. Educ., 2000, 77 (3), p 389
DOI: 10.1021/ed077p389
Publication Date (Web): March 1, 2000

Abstract

The construction of a simple automatic titrator is described. The buret is replaced with a metering pump to provide a constant flow of titrant. The output from the pH meter is sent to a recorder via a laboratory-constructed differentiator, allowing the results to be plotted as potential versus time, first or second derivative. The pump and recorder are plugged in to a standard power bar; turning the power bar on and off starts and stops the titration. Results obtained with the automatic titrator for the titration of sodium carbonate with HCl are as good as or better than those obtained with manual titration or commercial autotitrators.

Keywords (Audience):

First-Year Undergraduate / General

Keywords (Domain):

Analytical Chemistry

Keywords (Subject):

Instrumental Methods

Citing Articles

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This article has been cited by 2 ACS Journal articles (2 most recent appear below).

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    Comparing the Titrations of Mixed-Acid Solutions Using Dropwise and Constant-Flow Techniques

    Paul Charlesworth , Matthew J. Seguin and David J. Chesney
    Journal of Chemical Education2003 80 (11), 1311
    • Comparing the Titrations of Mixed-Acid Solutions Using Dropwise and Constant-Flow Techniques

      Paul Charlesworth , Matthew J. Seguin and David J. Chesney
      Journal of Chemical Education2003 80 (11), 1311

      A mixed-acid solution containing hydrochloric and phosphoric acids was used to determine the error associated with performing a real-time titration. The results were compared against those obtained by performing the titration in a more traditional ...

  • Cover Image

    Applied Electronics: Construction of a Simple Spectrophotometer

    Melissa A. Thal , Michael J. Samide
    Journal of Chemical Education2001 78 (11), 1510
    • Applied Electronics: Construction of a Simple Spectrophotometer

      Melissa A. Thal , Michael J. Samide
      Journal of Chemical Education2001 78 (11), 1510

      In this paper we describe the construction of a simple spectrophotometer intended for use as a capstone circuit for an electronics laboratory exercise. Students in the undergraduate laboratory have learned basic circuitry and are now able to read a ...

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History

  • Received: August 03, 2009

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