A Microscale Spectrophotometric Determination of Water Hardness

James S. Gordon , Stephanie Harman , Kristen Weiss and Brian Pettegrew
Division of Science, Central Methodist College, Fayette, MO 65248
J. Chem. Educ., 2001, 78 (8), p 1089
DOI: 10.1021/ed078p1089
Publication Date (Web): August 1, 2001

Abstract

A spectrophotometric titration was performed to determine water hardness. The titration incorporated the traditional titration method employing EDTA as the titrant and calmagite as the indicator. The microscale experiment was carried out in a spectrometer cuvette and made use of a Texas Instruments (TI-83) calculator interfaced through a TI Calculator-Based Laboratory system to a Vernier colorimeter as the detector. Monitoring at 635 nm, one of the colorimeter's fixed wavelengths, was well suited for this analysis. Agreement was found with results from traditional titrations.

Keywords (Audience):

First-Year Undergraduate / General

Keywords (Domain):

Analytical Chemistry

Keywords (Feature):

The Microscale Laboratory

Keywords (Pedagogy):

Hands-On Learning / Manipulatives

Keywords (Subject):

UV-Vis Spectroscopy

Citing Articles

Citation data is made available by participants in CrossRef's Cited-by Linking service. For a more comprehensive list of citations to this article, users are encouraged to perform a search in SciFinder.

This article has been cited by 7 ACS Journal articles (5 most recent appear below).

  • Cover Image

    Developing Technical Writing Skills in the Physical Chemistry Laboratory: A Progressive Approach Employing Peer Review

    Derek E. Gragson and John P. Hagen
    Journal of Chemical Education2010 87 (1), 62-65
    • Developing Technical Writing Skills in the Physical Chemistry Laboratory: A Progressive Approach Employing Peer Review

      Derek E. Gragson and John P. Hagen
      Journal of Chemical Education2010 87 (1), 62-65

      Writing formal “journal-style” lab reports is often one of the requirements chemistry and biochemistry students encounter in the physical chemistry laboratory. Helping students improve their technical writing skills is the primary reason this type of ...

  • Cover Image

    Teaching and Applying Chemistry-Specific Writing Skills Using a Simple, Adaptable Exercise

    Marin S. Robinson , Fredricka L. Stoller , Brad Horn and William Grabe
    Journal of Chemical Education2009 86 (1), 45
    • Teaching and Applying Chemistry-Specific Writing Skills Using a Simple, Adaptable Exercise

      Marin S. Robinson , Fredricka L. Stoller , Brad Horn and William Grabe
      Journal of Chemical Education2009 86 (1), 45

      We present a writing task designed to increase students' awareness of chemistry-specfic writing practices. This easy-to-use-and-grade task requires students to evaluate 10 short passages, a table, and a figure, representative of excerpts from Introduction,...

  • Cover Image

    Writing Across the Semester: A Non-Standard Term Paper That Encourages Critical Data Analysis in the Upper-Division Chemistry Classroom

    Jennifer Whiles Lillig
    Journal of Chemical Education2008 85 (10), 1392
    • Writing Across the Semester: A Non-Standard Term Paper That Encourages Critical Data Analysis in the Upper-Division Chemistry Classroom

      Jennifer Whiles Lillig
      Journal of Chemical Education2008 85 (10), 1392

      Scientific literacy is an important fundamental skill for scientists. In order for students to improve their writing they require constant feedback throughout the process. They also need to learn the value of the peer review process by experience. ...

  • Cover Image

    Using the ACS Journals Search To Validate Assumptions about Writing in Chemistry and Improve Chemistry Writing Instruction

    Marin S. Robinson , Fredricka L. Stoller and James K. Jones
    Journal of Chemical Education2008 85 (5), 650
    • Using the ACS Journals Search To Validate Assumptions about Writing in Chemistry and Improve Chemistry Writing Instruction

      Marin S. Robinson , Fredricka L. Stoller and James K. Jones
      Journal of Chemical Education2008 85 (5), 650

      This article illustrates how faculty and students can use the ACS Journals Search to examine assumptions about writing in chemistry. We examined common writing practices in chemistry including (i) the use of nominalizations, active and passive voice, and ...

  • Cover Image

    A Research-Based Laboratory Course in Organic Chemistry

    Thomas A. Newton , Henry J. Tracy and Caryn Prudenté
    Journal of Chemical Education2006 83 (12), 1844
    • A Research-Based Laboratory Course in Organic Chemistry

      Thomas A. Newton , Henry J. Tracy and Caryn Prudenté
      Journal of Chemical Education2006 83 (12), 1844

      The development, implementation, evolution, and evaluation of a unique approach to laboratory instruction in organic chemistry is described. The new course involves a multistep synthesis of group 14 metalloles. The program employs a combinatorial strategy ...

Tools

SciFinder Links

SciFinder subscribers:  Click to sign in | Not a SciFinder subscriber? Learn more at www.cas.org

Explore by:


History

  • Received: August 03, 2009

Recommend & Share

  • Share on ACS NetworkACS Network
  • Add to FacebookFacebook
  • Tweet ThisTweet This
  • Add to CiteULikeCiteULike
  • Add to NewsvineNewsvine
  • Digg ThisDigg This
  • Add to DeliciousDelicious

Related Content