Article
Constructing a High-Sensitivity, Computer-Interfaced, Differential Thermal Analysis Device for Teaching and Research
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Abstract
We report the construction of a homemade differential thermal analysis instrument interfaced with a computer through a data acquisition board and handled with a program written in LabVIEW. This instrument has been used for teaching purposes, in the construction of phase diagrams, and for research purposes, particularly to measure glass transition temperatures because of its demonstrated sensitivity. Constructing this instrument serves as an excellent opportunity to help students understand the basic elements of analytical instrumentation and as a simple way of introducing them to digital data acquisition and computer interfacing, which are important skills for modern chemists.
Keywords (Audience):
General PublicKeywords (Domain):
Analytical ChemistryKeywords (Pedagogy):
Computer-Based LearningKeywords (Subject):
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This article has been cited by 1 ACS Journal articles (1 most recent appear below).

Fast and Slow Components in the Crystallization of a Model Multicomponent System, NaKCa(NO3): The Role of Composition Fluctuations
Ping Wen and Peter Harrowell , C. Austen AngellThe Journal of Physical Chemistry A2011 115 (23), 6260-6268Fast and Slow Components in the Crystallization of a Model Multicomponent System, NaKCa(NO3): The Role of Composition Fluctuations
Ping Wen and Peter Harrowell , C. Austen AngellThe Journal of Physical Chemistry A2011 115 (23), 6260-6268We use calorimetrically detected crystal nucleation and growth studies to broaden the discussion of fluctuation-induced nucleation processes to include composition fluctuations in ionic complex-forming systems. We use the model system Ca(NO3)2–KNO3 with ...
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History
- Received: August 03, 2009
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