Facile Synthesis of Tin Oxide Nanoparticles Stabilized by Dendritic Polymers

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Abstract

Tin(IV) oxide nanoparticles were synthesized via the reaction of carbon dioxide with stannate ions immobilized by dendritic polymers. For PAMAM and PPI dendrimer hosts, resultant nanoparticle diameters were 2.5−3 nm; 3−3.5 nm nanoparticles resulted from use of a poly(ethyleneimine) hyperbranched polymer. Our conditions represent the only precedent for SnO₂ nanoparticulate growth using dendritic architectures, as well as a novel application for CO₂ as a reactive gas for the controlled growth of metal oxide nanoparticles.

Citing Articles

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This article has been cited by 16 ACS Journal articles (5 most recent appear below).

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  Synthesis of SnO₂ Hierarchical Structures Assembled from Nanosheets and Their Lithium Storage Properties

  Hao Bin Wu, Jun Song Chen, Xiong Wen (David) Lou, and Huey Hoon Hng
  The Journal of Physical Chemistry C2011 115 (50), 24605-24610

  • Synthesis of SnO₂ Hierarchical Structures Assembled from Nanosheets and Their Lithium Storage Properties

    Hao Bin Wu, Jun Song Chen, Xiong Wen (David) Lou, and Huey Hoon Hng
    The Journal of Physical Chemistry C2011 115 (50), 24605-24610

    In this work, we have developed a facile hydrothermal method to synthesize various 3D hierarchical structures assembled from 2D SnO2 nanosheets. The samples were thoroughly characterized by FESEM/TEM/XRD/BET techniques. Through in-depth investigation of ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Tin(IV) Oxide Coatings from Hybrid Organotin/Polymer Nanoparticles

  Rafael Muñoz-Espí, Paolo Dolcet, Torsten Rossow, Manfred Wagner, Katharina Landfester, and Daniel Crespy
  ACS Applied Materials & Interfaces2011 3 (11), 4292-4298

  • Tin(IV) Oxide Coatings from Hybrid Organotin/Polymer Nanoparticles

    Rafael Muñoz-Espí, Paolo Dolcet, Torsten Rossow, Manfred Wagner, Katharina Landfester, and Daniel Crespy
    ACS Applied Materials & Interfaces2011 3 (11), 4292-4298

    Tin dioxide coatings are widely applied in glasses and ceramics to improve not only optical, but also mechanical properties. In this work, we report a new method to prepare SnO2 coatings from aqueous dispersions of polymer/organotin hybrid nanoparticles. ...

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• 

  Dendrimers as Encapsulating, Stabilizing, or Directing Agents for Inorganic Nanoparticles

  Lyudmila M. Bronstein and Zinaida B. Shifrina
  Chemical Reviews2011 Article ASAP

  • Dendrimers as Encapsulating, Stabilizing, or Directing Agents for Inorganic Nanoparticles

    Lyudmila M. Bronstein and Zinaida B. Shifrina
    Chemical Reviews2011 Article ASAP
    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Antimony Tin Oxide (ATO) Nanoparticle Formation from H₂O₂ Solutions: a New Generic Film Coating from Basic Solutions

  Sergey Sladkevich, Alexey A. Mikhaylov, Petr V. Prikhodchenko, Tatiana A. Tripol’skaya, and Ovadia Lev
  Inorganic Chemistry2010 49 (20), 9110-9112

  • Antimony Tin Oxide (ATO) Nanoparticle Formation from H₂O₂ Solutions: a New Generic Film Coating from Basic Solutions

    Sergey Sladkevich, Alexey A. Mikhaylov, Petr V. Prikhodchenko, Tatiana A. Tripol’skaya, and Ovadia Lev
    Inorganic Chemistry2010 49 (20), 9110-9112

    A generic method for conductive film coating of minerals and acid-sensitive materials by antimony-doped tin oxide (ATO) is introduced. The coating was performed from a hydrogen peroxide stabilized stannate and antimonate precursor solution. This is the ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links
• 

  Interaction of Alkaline Metal Cations with Oxidic Surfaces: Effect on the Morphology of SnO₂ Nanoparticles

  Alexander Birkel, Niklas Loges, Enrico Mugnaioli, Robert Branscheid, Dominik Koll, Stefan Frank, Martin Panthöfer and Wolfgang Tremel
  Langmuir2010 26 (5), 3590-3595

  • Interaction of Alkaline Metal Cations with Oxidic Surfaces: Effect on the Morphology of SnO₂ Nanoparticles

    Alexander Birkel, Niklas Loges, Enrico Mugnaioli, Robert Branscheid, Dominik Koll, Stefan Frank, Martin Panthöfer and Wolfgang Tremel
    Langmuir2010 26 (5), 3590-3595

    Reaction pathways to SnO2 nanomaterials through the hydrolysis of hydrated tin tetrachloride precursors were investigated. The products were prepared solvothermally starting from hydrated tin tetrachloride and various (e.g., alkali) hydroxides. The ...

    Abstract | Full Text HTML | Hi-Res PDF | PDF w/ Links

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