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Pd/C as a Reusable Catalyst for the Coupling Reaction of Halophenols and Arylboronic Acids in Aqueous Media
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Abstract
Pd/C was found to catalyze the Suzuki−Miyaura coupling reaction of halophenols in aqueous media. When halophenols were treated with ArB(OH)2 and a catalytic amount of 10% Pd/C (0.3 mol % Pd) in aqueous K2CO3 solution, the corresponding hydroxybiaryls were obtained in a high yield or quantitatively. The palladium catalyst was easily recovered and reused.
Citing Articles
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This article has been cited by 36 ACS Journal articles (5 most recent appear below).
Efficient Screening and Library Generation in Parallel C–C Coupling Reactions Mediated by Organosilica SiliaCat Palladium Catalysts
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Valerica Pandarus, Genevieve Gingras, François Béland, Rosaria Ciriminna, and Mario PagliaroOrganic Process Research & Development2012 16 (1), 117-122Organosilica SiliaCat palladium catalysts applied to the conversion of widely different substrates in Suzuki, Sonogashira, and Heck coupling reactions run in a parallel synthesizer enable quick screening of the reaction system with identification of the ...
Efficient, Selective, and Recyclable Palladium Catalysts in Carbon−Carbon Coupling Reactions
Árpád MolnárChemical Reviews2011 111 (3), 2251-2320Efficient, Selective, and Recyclable Palladium Catalysts in Carbon−Carbon Coupling Reactions
Árpád MolnárChemical Reviews2011 111 (3), 2251-2320
Large-Scale Applications of Transition Metal-Catalyzed Couplings for the Synthesis of Pharmaceuticals
Javier Magano and Joshua R. DunetzChemical Reviews2011 111 (3), 2177-2250Large-Scale Applications of Transition Metal-Catalyzed Couplings for the Synthesis of Pharmaceuticals
Javier Magano and Joshua R. DunetzChemical Reviews2011 111 (3), 2177-2250
Practical Aspects of Carbon−Carbon Cross-Coupling Reactions Using Heteroarenes
Vincent F. Slagt, André H. M. de Vries, Johannes G. de Vries and Richard M. KelloggOrganic Process Research & Development2010 14 (1), 30-47Practical Aspects of Carbon−Carbon Cross-Coupling Reactions Using Heteroarenes
Vincent F. Slagt, André H. M. de Vries, Johannes G. de Vries and Richard M. KelloggOrganic Process Research & Development2010 14 (1), 30-47The use of cross-coupling reactions for the preparation of alkylated and arylated heteroaromatic compounds has increased tremendously over the past two decades. This has been driven on the one hand by the increasingly complex structures of new drugs, most ...
Palladium Nanoparticles on Graphite Oxide and Its Functionalized Graphene Derivatives as Highly Active Catalysts for the Suzuki−Miyaura Coupling Reaction
Gil M. Scheuermann, Luigi Rumi, Peter Steurer, Willi Bannwarth and Rolf MülhauptJournal of the American Chemical Society2009 131 (23), 8262-8270Palladium Nanoparticles on Graphite Oxide and Its Functionalized Graphene Derivatives as Highly Active Catalysts for the Suzuki−Miyaura Coupling Reaction
Gil M. Scheuermann, Luigi Rumi, Peter Steurer, Willi Bannwarth and Rolf MülhauptJournal of the American Chemical Society2009 131 (23), 8262-8270Pd2+-exchanged graphite oxide and chemically derived graphenes therefrom were employed as supports for Pd nanoparticles. The influence of catalyst preparation, carbon functionalization, and catalyst morphology on the catalytic activity in the Suzuki−...
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History
- Published In Issue April 19, 2002
- Received December 3, 2001
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