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Efficient Synthesis of Salicylates by Catalytic [3 + 3] Cyclizations of 1,3-Bis(silyl enol ethers) with 1,1,3,3-Tetramethoxypropane

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Muhammad Sher,^†^‡ T. H. Tam Dang,^†^‡ Zafar Ahmed,^†^‡ Muhammad A. Rashid,^† Christine Fischer,^†^‡ and Peter Langer*^†^‡

Institut für Chemie, Universität Rostock, Albert-Einstein-Str. 3a, 18059 Rostock, Germany, and Leibniz-Institut für Katalyse e. V. an der Universität Rostock, Albert-Einstein-Str. 29a, 18059 Rostock, Germany peter.langer@uni-rostock.de

J. Org. Chem., 2007, 72 (16), pp 6284–6286

DOI: 10.1021/jo070974a

Publication Date (Web): July 13, 2007

Section:

Benzene, Its Derivatives, and Condensed Benzenoid Compounds

Abstract

Salicylic acid derivatives were prepared by Me₃SiOTf-catalyzed [3 + 3] cyclization of 1,3-bis(silyl enol ethers) with 1,1,3,3-tetramethoxypropane.

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