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Monodisperse Platinum Nanospheres with Adjustable Diameters from 10 to 100 nm: Synthesis and Distinct Optical Properties

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Institut für Physikalische Chemie und Elektrochemie, TU Dresden, Bergstr. 66 b, 01062 Dresden, Germany Institut für Angewandte Photophysik, TU Dresden, George-Bähr-Str. 1, 01069 Dresden, Germany Max-Planck-Institut für Chemische Physik fester Stoffe, Nöthnitzer Strasse 40, 01187 Dresden, Germany
* Corresponding author, [email protected]
†Institut für Physikalische Chemie and Elektrochemie, TU Dresden.
‡Institut für Angewandte Photophysik, TU Dresden.
§Max-Planck-Institut für Chemische Physik fester Stoffe.
Cite this: Nano Lett. 2008, 8, 12, 4588–4592
Publication Date (Web):November 5, 2008
https://doi.org/10.1021/nl802901t
Copyright © 2008 American Chemical Society
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    Abstract

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    We present a facile and reproducible method for synthesizing monodisperse platinum (Pt) spheres with sizes ranging from 10 to 100 nm in diameter and exceptionally small standard deviations of 3% for large spheres. The reaction takes place in aqueous solution using a multistep seed-mediated approach. The Pt nanospheres consist of several small crystallites resulting in a surface roughness of 5−10 nm. Extinction spectra are measured from particles dispersed in water and calculated for single particles which are found to be in excellent agreement. We obtain a linear correlation between the plasmon extinction maximum (from UV to the visible regions) and the particle diameter which might be of value for experimentalists in the field.

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    TEM micrographs of the platinum seeds and of the synthesized platinum spheres and a detailed theoretical description concerning the modeling of the extinction properties of these particles. This material is available free of charge via the Internet at http://pubs.acs.org.

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