Table of Contents

July 2008
Volume 85, Issue 7
Pages 891-1008

About the Cover:

Annatto Seeds in the Laboratory. The main compound of annatto seeds, bixin, has antioxidant properties and an orange-red color, which makes annatto extract useful in the cosmetic and food industries. In the article by Teixeira, Durán, and Guterres, students encapsulate bixin in poly(3-hydroxybutyrate-co-3-hydroxyvalerate) particles by an emulsion–solvent evaporation method, which involves colloidal chemistry concepts such as surface tension, emulsion stability, and Ostwald ripening. McCullagh and Ramos discuss the separation of bixin from annatto seeds using column chromatography. In the experiment students isolate significant quantities of the carotenoid from small quantities of plant material and learn how to choose the appropriate solvent for a chromatographic separation by analyzing several potential solvents using thin-layer chromatography. Annatto seed components are also the JCE Featured Molecules for July.

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Chemical Education Today

Energy

p 891
Publication Date (Web): July 1, 2008 (Editorial)
DOI: 10.1021/ed085p891
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Water Filtration: Small Changes Make a Difference

p 892
Publication Date (Web): July 1, 2008 (Communication)
DOI: 10.1021/ed085p892

Pizza, Flowers, and Fish

p 893
Publication Date (Web): July 1, 2008 (Editorial)
DOI: 10.1021/ed085p893
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Hiring and Promotion in Chemical Education

p 898
Publication Date (Web): July 1, 2008 (Report)
DOI: 10.1021/ed085p898

Teaching Chemistry in Graduate School

p 902
Publication Date (Web): July 1, 2008 (Commentary)
DOI: 10.1021/ed085p902
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Summer Reading

p 904
Publication Date (Web): July 1, 2008 (Commentary)
DOI: 10.1021/ed085p904
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Potassium Iodate

p 910
Publication Date (Web): July 1, 2008 (Communication)
DOI: 10.1021/ed085p910

Manganese(II) Sulfate

p 911
Publication Date (Web): July 1, 2008 (Communication)
DOI: 10.1021/ed085p911

News and Announcements

p 913
Publication Date (Web): July 1, 2008 (News and Announcements)
DOI: 10.1021/ed085p913
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Modification to Synthesis of Methyl Diantilis

p 917
Publication Date (Web): July 1, 2008 (Letter)
DOI: 10.1021/ed085p917.1
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Hydrophobic Solvation NOT via Clathrate Water Cages

p 917
Publication Date (Web): July 1, 2008 (Letter)
DOI: 10.1021/ed085p917.2
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Hydrophobic Solvation NOT via Clathrate Water Cages

p 918
Publication Date (Web): July 1, 2008 (Letter)
DOI: 10.1021/ed085p918
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Introduction to Quantum Mechanics: A Time-Dependent Perspective (David J. Tannor)

p 919
Publication Date (Web): July 1, 2008 (Book and Media Review)
DOI: 10.1021/ed085p919
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Chemistry for Everyone

If You Were a Molecule in a Chromatography Column, What Would You See?

p 925
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p925

In the Classroom

A Model for Incorporating Research into the First-Year Chemistry Curriculum

p 929
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p929

Presentation and Impact of Experimental Techniques in Chemistry

p 934
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p934

In the Laboratory

The Resolution of Ibuprofen, 2-(4'-Isobutylphenyl)propionic Acid

p 941
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p941

The Preparation and Enzymatic Hydrolysis of a Library of Esters

p 944
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p944

Annatto Polymeric Microparticles: Natural Product Encapsulation by the Emulsion–Solvent Evaporation Method

p 946
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p946

Separation of the Carotenoid Bixin from Annatto Seeds Using Thin-Layer and Column Chromatography

p 948
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p948

Quantification of Tea Flavonoids by High Performance Liquid Chromatography

p 951
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p951

HPLC Analysis of α- and β-Acids in Hops

p 954
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p954

Determination of Cinnamaldehyde in Cinnamon by SPME–GC–MS. An Instrumental Analysis Experiment

p 957
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p957

Evaluating Mechanisms of Dihydroxylation by Thin-Layer Chromatography. A Microscale Experiment for Organic Chemistry

p 959
Publication Date (Web): July 1, 2008 (Lab-Expt)
DOI: 10.1021/ed085p959

The Iodochlorination of Styrene: An Experiment That Makes a Difference

p 962
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p962

Using Single Drop Microextraction for Headspace Analysis with Gas Chromatography

p 965
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p965

Measurement of Henry's Law Constants Using Internal Standards. A Quantitative GC Experiment for the Instrumental Analysis or Environmental Chemistry Laboratory

p 969
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p969

Teaching Sustainable Development Concepts in the Laboratory: A Solid–Liquid Extraction Experiment

p 972
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p972

An Environmentally Friendly, Cost-Effective Determination of Lead in Environmental Samples Using Anodic Stripping Voltammetry

p 976
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p976

Sampling the Soils Around a Residence Containing Lead-Based Paints: An X-ray Fluorescence Experiment

p 980
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p980

Research: Science and Education

Understanding Why Researchers Should Use Synchrotron-Enhanced FTIR Instead of Traditional FTIR

p 983
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p983

Peer-Led Team Learning in General Chemistry: Implementation and Evaluation

p 990
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p990

On the Web

Teaching Chemistry Students How To Use Patent Databases and Glean Patent Information

p 997
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p997

Developing and Disseminating NOP: An Online, Open-Access, Organic Chemistry Teaching Resource To Integrate Sustainability Concepts in the Laboratory

p 1000
Publication Date (Web): July 1, 2008 (Article)
DOI: 10.1021/ed085p1000

JCE Classroom Activities #1–50, on CD-ROM

p 1006
Publication Date (Web): July 1, 2008 (Tech Report)
DOI: 10.1021/ed085p1006
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Molecular Models of Annatto Seed Components

p 1008
Publication Date (Web): July 1, 2008 (Tech Report)
DOI: 10.1021/ed085p1008
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