Table of Contents

November 1963
Volume 28, Issue 11
Pages 2937-3274
For Selected Content:

Articles

Bridged Lactones and Bridged Carbocyclic Systems from 2-(3,4,5-Trimethoxyphenyl)-4,5-dimethyl-Δ4-cyclohexenecarboxylic Acid. Novel Mescaline Analogs1

pp 2937–2943
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a001
ACS Legacy Archive

Studies Directed toward the Total Synthesis of Azasteroids. I. 3,4-Cyclopenteno-5,6-dihydropyridines and 6,6-Tetramethylene-5,6-dihydro-1,3-oxazines1-3

pp 2944–2950
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a002
ACS Legacy Archive

Studies Directed toward the Total Synthesis of Azasteroids. II. Cyclopenteno[d]-1-azabicycloalkanes as Precursors to Azasteroids1,2

pp 2950–2953
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a003
ACS Legacy Archive

The Mechanism of Azo Ester Addition—Abstraction Reactions with Cyclic Dienes

pp 2954–2960
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a004
ACS Legacy Archive

Synthesis of Bicyclic Nitriles and Related Compounds. II1,2

pp 2960–2965
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a005
ACS Legacy Archive

Bicyclo[2.2.2]octane-1,2-dicarboxylic Acid1

pp 2965–2970
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a006
ACS Legacy Archive

The Lactones of cis- and trans-2-Hydroxycycloheptaneacetic Acid1

pp 2970–2975
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a007
ACS Legacy Archive

The Reactions of Phosphonic Acid Esters with Acid Chlorides. A Very Mild Hydrolytic Route

pp 2975–2978
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a008
ACS Legacy Archive

The Ammonolysis of 1,6-Anhydro-2,4-di-O-p-tolylsulfonyl-β-D-glucopyranose and the Synthesis of 2,4-Diamino-2,4-dideoxy-D-glucose1

pp 2978–2983
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a009
ACS Legacy Archive

Glycosyl Halide Derivatives of 3-Amino-3-deoxy-D-mannose1

pp 2989–2992
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a012
ACS Legacy Archive

Conversion of 2-Amino-2-deoxy-1-thio-D-glucose Derivatives into Glycosyl Halide Derivatives. A Tetra-O-acetylglycosylsulfenyl Bromide1

pp 2992–2995
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a013
ACS Legacy Archive

Preparation of Some trans-Aminomercaptofuranose Sugars1

pp 2995–2999
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a014
ACS Legacy Archive

Syntheses with Partially Benzylated Sugars. III.1 A Simple Pathway to a “cis- Nucleoside,” 9-β-D-Arabinofuranosyladenine (Spongoadenosine)

pp 3004–3006
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a016
ACS Legacy Archive

On the Barrier to Inversion of Cyclooctatetraene. The Thermal Decomposition of Dibenzo[e,g][1,4]diazocine1

pp 3007–3010
Publication Date: November 1963 (Article)
DOI: 10.1021/jo01046a017
ACS Legacy Archive

The Rearrangement of 2-Amino-5-phenyl-3H-1,4-benzodiazepine 4-Oxides with Acetic Anhydride

pp 3010–3012
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a018
ACS Legacy Archive

Quinazolines and Benzodiazepines. XV.1 7-Nitro- and 7-Trifluoromethyl-2,3-dihydro-5-phenyl-1H-1,4-benzodiazepines and Their Transformations

pp 3013–3016
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a019
ACS Legacy Archive

Reactions of Metal Chelates. VI.1,2 The Synthesis and Reactions of a Stable Chelate Diazonium Salt3

pp 3017–3021
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a020
ACS Legacy Archive

Aldehyde Hemihydrates

pp 3029–3034
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a023
ACS Legacy Archive

The Addition of Aromatic Nitroso Compounds to Conjugated Dienes

pp 3034–3036
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a024
ACS Legacy Archive

Free Radical Addition of Cyclic Ethers to Maleic Anhydride

pp 3036–3038
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a025
ACS Legacy Archive

Pyrimido[5,4-e]-as-triazines. II. The Preparation and Reactions of Some Heteroaromatic 5-Aminopyrimido[5,4-e]-as-triazines1

pp 3038–3041
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a026
ACS Legacy Archive

Aromaticity in Heterocyclic Systems. I. The Synthesis and Structure of Certain 4,6-Dihydroxyimidazo[4,5-c]pyridines1

pp 3041–3046
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a027
ACS Legacy Archive

The Conversion of 3-Aminoalkylidene-2,4-pyrandiones into 4-Pyridones

pp 3046–3049
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a028
ACS Legacy Archive

Concerning the Position of Thiocyanation in Pyrrole1

pp 3050–3052
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a029
ACS Legacy Archive

The Methylpyrroles. Synthesis and Characterization

pp 3052–3058
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a030
ACS Legacy Archive

Arrested Deamination in the Fischer Indole Synthesis. The Synthesis of 1,2,3,3a,4,8b-Hexahydropyrrolo[3,4-b]indoles with Angular Substitution1

pp 3058–3065
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a031
ACS Legacy Archive

Aromatic Cyclodehydration. LIV.1 Indolo[2,3-a]acridizinium Salts

pp 3070–3072
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a033
ACS Legacy Archive

The Solvolysis of 4α- and 4β-Methylcholesteryl p-Toluenesulfonate1a

pp 3072–3077
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a034
ACS Legacy Archive

Electrophilic Substitution of the Benzenethiols. II. Acylbenzene- and Acyltoluenethiols1,2

pp 3077–3082
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a035
ACS Legacy Archive

The Reaction between Acenaphthenequinone and Phenyllithium

pp 3082–3084
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a036
ACS Legacy Archive

The Synthesis and Properties of n-Octane-d18 and 2,2,4-Trimethylpentane-d181

pp 3085–3087
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a037
ACS Legacy Archive

Syntheses of α-Keto Amides and Acids from Ethyl Alkylidenecyanoacetates1

pp 3088–3092
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a038
ACS Legacy Archive

1-Iodo-2-(perfluoroalkyl)cycloalkanes by the Free Radical Addition of Iodoperfluoroalkanes to Cyclohexane and Cyclopentene

pp 3093–3102
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a039
ACS Legacy Archive

Some Chemical Transformations and Conformations in the Cycloheptadecanone Series1

pp 3103–3107
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a040
ACS Legacy Archive

Alkylations of Phenylacetic Esters with Halides by Means of Sodium Amide in Liquid Ammonia. Comparisons with Alkylations of Phenylacetic Acid1a

pp 3108–3112
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a041
ACS Legacy Archive

Ethylenediketene Dimer

pp 3112–3114
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a042
ACS Legacy Archive

The Ferric Chloride Oxidation of 5-Substituted o-Semidines and the Polarographic Properties of the Products

pp 3114–3120
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a043
ACS Legacy Archive

The Estimation of Hammett Substituent Constants1

pp 3121–3124
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a044
ACS Legacy Archive

Thiolesters by Anhydride Reduction with Hydrogen Sulfide

pp 3124–3129
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a045
ACS Legacy Archive

2-Amino-5,6-dihydro-1,3-oxazines. The Reduction of Carboxylic Esters with Sodium Borohydride1

pp 3129–3134
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a046
ACS Legacy Archive

Reactions of Acetylenic Esters with Enamines

pp 3134–3140
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a047
ACS Legacy Archive

Reactions of Mercaptoamines. I. With Isocyanates and Isothiocyanates1

pp 3140–3144
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a048
ACS Legacy Archive

The Dealkylation of Aromatic Amines

The Dealkylation of Aromatic Amines

pp 3144–3147
Publication Date: November 1963 (Article)
DOI: 10.1021/jo01046a049
ACS Legacy Archive

The Swamping Catalyst Effect. V. The Halogenation of Aromatic Acid Derivatives1

pp 3147–3149
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a050
ACS Legacy Archive

Structure of the 2:2 Condensation Product of Nitromethane and Cyclohexanone

pp 3150–3165
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a051
ACS Legacy Archive

Hydrocarbon Chlorinations with Phosphorus Pentachloride1

pp 3173–3177
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a053
ACS Legacy Archive

The Reaction of Ethyl Azodicarboxylate with Conjugated Dienes. II1,2

pp 3177–3181
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a054
ACS Legacy Archive

The Reduction of Acid Adducts of Isoquinoline Reissert Compounds1

pp 3181–3184
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a055
ACS Legacy Archive

Deoxymercuration in the Presence of Both Acid and Iodide Ion1

pp 3184–3188
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a056
ACS Legacy Archive

Reactions of Aromatic Carboxylates. I. Evidence for the Intermediacy of Benzyne in the Pyrolyses of o-Halobenzoates1

pp 3188–3194
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a057
ACS Legacy Archive

Fate of the Carbinol Carbon in the Conversion of Tetrahydrofurfuryl Alcohol to Dihydropyran

pp 3194–3197
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a058
ACS Legacy Archive

A Steroidal Internal Displacement Reaction1

pp 3197–3199
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a059
ACS Legacy Archive

Organoboron Compounds. XVII.1 Chemistry of a Compound with Neighboring Borono, Ethynyl, and Amine Functional Groups2

pp 3199–3202
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a060
ACS Legacy Archive

Notes

pp 3202–3274
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a061
ACS Legacy Archive

Reduction of 1-Methyl-3-acylindole Derivatives with Lithium Aluminum Hydride1

pp 3202–3205
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a501
ACS Legacy Archive

Aromatic Cyclodehydration. LV.1 Quaternizations with Chloroacetaldoxime

pp 3205–3206
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a502
ACS Legacy Archive

The Hoesch Condensation of Dihydro-β-tubanol with Benzyl Cyanides

pp 3206–3208
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a503
ACS Legacy Archive

The Mechanism of Dehydration of β,β-Diphenyl-β-hydroxypropiophenone1

pp 3208–3209
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a504
ACS Legacy Archive

Investigations in Heterocycles. XIV. 2- and 3-Azaoctahydroindolo[2,3a]quinolizines1

pp 3210–3212
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a506
ACS Legacy Archive

A Synthesis of 6-Methyl-2-phenyl-5-azacycl[3.2.2]azine and Related Compounds1,2

pp 3212–3213
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a507
ACS Legacy Archive

Synthesis and Polymerization of 3-Azabicyclo-[4.3.1]decan-4-one and 7,7-Dimethyl-2-azabicyclo[4.1.1]octan-3-one

pp 3213–3214
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a508
ACS Legacy Archive

Products from the Acetolysis of (-)-(S)-Bicyclo[2.2.2.]octyl-2 p-Bromobenzenesulfonate. A Reinvestigation1

pp 3214–3216
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a509
ACS Legacy Archive

Nuclear Magnetic Resonance Identification of Substitutional Isomers in Chelated Polycyclic Aromatic Systems1

pp 3216–3217
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a510
ACS Legacy Archive

trans-5-Cyclodecenone1

pp 3217–3219
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a511
ACS Legacy Archive

cis- and trans-1,2,3-Tricyanocyclopropanes

pp 3219–3220
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a512
ACS Legacy Archive

1,5-Dimethyl-2-oxo-3-pyrrolidineglyoxylic Acid

pp 3221–3222
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a513
ACS Legacy Archive

Synthesis and Characterization of Some Toluides of o-Phthalic Acid

pp 3223–3225
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a514
ACS Legacy Archive

F19 Nuclear Magnetic Resonance Spectra of Some Benzotrifluorides

p 3225
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a515
ACS Legacy Archive

Proton Nuclear Magnetic Resonance Analysis of Some Acylmetallocenes

pp 3225–3228
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a516
ACS Legacy Archive

The Synthesis of a Glucosamine—Asparagine Compound. Benzyl N2-Carbobenzyloxy-N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-L-asparaginate1

pp 3228–3230
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a517
ACS Legacy Archive

A Convenient Preparation of 1,2-Mono-O-isopropylidene-α-D-glucofuranose1

pp 3230–3231
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a518
ACS Legacy Archive

3,4,6-Tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl Bromide Hydrobromide1

pp 3231–3232
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a519
ACS Legacy Archive

The Chromous Chloride Reduction of Ergosterol Epidioxide1

pp 3232–3234
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a520
ACS Legacy Archive

The Reactions of Nortricyclyl and Dehydronorbornyl Chloride with Sodium

pp 3234–3237
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a521
ACS Legacy Archive

Reaction of α,ι-Dienes with Diisobutylaluminum Hydride

pp 3237–3238
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a522
ACS Legacy Archive

Ferrocenes. VI. Oxidation in Friedel—Crafts Reactions1,2

pp 3238–3240
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a523
ACS Legacy Archive

o-Nitrosobenzamide. A Possible Intermediate in the von Richter Reaction

pp 3240–3241
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a524
ACS Legacy Archive

Amines Derived from Dihalopropenes. V.1a Reaction of 2-Haloallylamines with Various Bases1b

pp 3241–3243
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a525
ACS Legacy Archive

Dihalomalonaldehydes

pp 3243–3245
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a526
ACS Legacy Archive

Effect of Solvent Composition on the Kinetics of the Cyanoethylation of Methanol

pp 3245–3246
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a527
ACS Legacy Archive

Oxidation of Thiols by Dimethyl Sulfoxide

pp 3246–3248
Publication Date: November 1963 (Article)
DOI: 10.1021/jo01046a528
ACS Legacy Archive

The Jacobsen Rearrangement of 6-Methyl-7-propyltetralin1

pp 3248–3249
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a529
ACS Legacy Archive

An Extention of the Gomberg—Bachmann Pinacol Synthesis

pp 3249–3250
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a530
ACS Legacy Archive

Ring Expansion and Electron Transfer in the Cleavage of 2,2'-Diphenyl-2,2'-biindan-1,1',3,3'-tetrone with Base1

pp 3250–3252
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a531
ACS Legacy Archive

The Photochemical Conversion of Phenyl Isocyanate and Diphenyldiazomethane to 2,2-Diphenylindoxyl

pp 3252–3253
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a532
ACS Legacy Archive

The Synthesis of Naphtho[2,1-a]perylene and Dibenzo[ae]perylene1,2

pp 3253–3255
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a533
ACS Legacy Archive

α-Hydroxy Acid Amides. A Convenient Synthesis

pp 3255–3256
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a534
ACS Legacy Archive

The Brominating Properties of Tetramethylammonium Tribromide1a

pp 3256–3258
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a535
ACS Legacy Archive

The Reaction of Secondary Amines with Formaldehyde

pp 3258–3259
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a536
ACS Legacy Archive

The Synthesis of Secondary and Tertiary Amines by Borohydride Reduction1

The Synthesis of Secondary and Tertiary Amines by Borohydride Reduction1

pp 3259–3261
Publication Date: November 1963 (Article)
DOI: 10.1021/jo01046a537
ACS Legacy Archive

The Reduction of Esters with Sodium Borohydride1

pp 3261–3263
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a538
ACS Legacy Archive

Optically Active Benzylamine-α-d1

pp 3263–3264
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a539
ACS Legacy Archive

Organosilicon and Tin Alkylthiols

pp 3264–3266
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a540
ACS Legacy Archive

A Hammett Study of Hydrogen Abstraction from Substituted Allylbenzenes

pp 3266–3267
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a541
ACS Legacy Archive

Derivatives of 2-Benzyl-1-indanone. Competing Alicyclic and Aromatic Monobromination

pp 3267–3269
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a542
ACS Legacy Archive

A Convenient Method for Utilizing the Allyl Grignard Reagent

pp 3269–3272
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a543
ACS Legacy Archive

Rates and Relative Rates of Chloro- and Iododesilylation. Evidence for a Four-Center Transition State

pp 3272–3274
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a544
ACS Legacy Archive

The Isolation of a New Diterpene Acid

p 3274
Publication Date: November 1963 ()
DOI: 10.1021/jo01046a545
ACS Legacy Archive
For Selected Content:
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