The Journal of Organic Chemistry: Volume 29, Issue 11 (ACS Publications)

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November 1964

Volume 29, Issue 11

Pages 3133-3452

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Articles

The Linear Relationship between Enthalpy and Entropy of Activation

Raymond C. Petersen

pp 3133–3135

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a001

First Page

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The Effect of Axial Alkyl Groups on the Base Strengths of Cyclic Amines

H. K. Hall Jr.

pp 3135–3138

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a002

First Page

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Anomalous Reduction of 2,2,4,4-Tetramethylcyclobutane-1,3-dioxime by Lithium Aluminum Hydride

H. K. Hall Jr.

pp 3139–3143

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a003

First Page

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The Mechanism and Stereochemistry of Formation and Cleavage of Epoxy Ethers. I^2,3

Theodore B. Zalucky, Louis Malspeis, Gilbert Hite

pp 3143–3146

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a004

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Epoxy Ethers. XX.¹ Synthesis of Diamines, Morpholines, and Piperazines

Calvin L. Stevens, Morton E. Munk, Charles H. Chang, K. Grant Taylor, Alfred L. Schy

pp 3146–3151

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a005

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A Study of the Aminophthalimidoacetic Acids¹

Lyman R. Caswell, Patsey C. Atkinson

pp 3151–3154

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a006

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The Syntheses of cis- and trans-Δ⁴-Tetrahydrohomophthalic Acids

F. V. Brutcher Jr., D. D. Rosenfeld

pp 3154–3158

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a007

First Page

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The Configuration at C-20 of 11-Oxygenated 3α,20-Dihydroxy-5β-pregnan-21-oic Acids¹

Vernon R. Mattox, Wiley Vrieze

pp 3158–3161

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a008

First Page

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The Synthesis of 3-Alkoxy-cis-2-trans-4-unsaturated Acids¹

Edward E. Smissman, A. Nelson Voldeng

pp 3161–3165

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a009

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Synthesis of a Homolog of Aspergillic Acid

Mitsuo Masaki, Masaki Ohta

pp 3165–3168

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a010

First Page

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Synthesis of ortho and meta Analogs of Thyropropionic Acid and of Their Iodinated Derivatives¹

Teruo Matsuura, Akira Nishinaga

pp 3168–3170

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a011

First Page

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Synthesis of meta Analogs of Thyroxine

Tetsuo Shiba, Annemarie Höfer, H. J. Cahnmann

pp 3171–3175

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a012

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Synthesis of 2:3-Benzo-1-silacycloalkenes. I

Henry Gilman, Oren L. Marrs

pp 3175–3179

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a013

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Cyclizations of Dialdehydes with Nitromethane. XII.¹ o-Phthalaldehyde²

Hans Helmut Baer, Barbara Achmatowicz

pp 3180–3185

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a014

First Page

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Stereochemistry and Mechanism of Lithium Aluminum Hydride and Mixed Hydride Reduction of 4-t-Butylcyclohexene Oxide¹

Bruce Rickborn, Joe Quartucci

pp 3185–3188

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a015

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Cleavage of 1,2-Diazetidinones by Bases. The Reaction of 1,2,4,4-Tetraphenyl-1,2-diazetidinone with Alkoxides, Organolithium Compounds, and Lithium Aluminum Hydride

J. Herbert Hall

pp 3188–3191

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a016

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Perchloro Cage Compounds. I. Structural Studies¹

G. W. Griffin, A. K. Price

pp 3192–3196

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a017

First Page

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Thiazoline and Oxazoline Hydrolyses and Sulfur-Nitrogen and Oxygen-Nitrogen Acyl Transfer Reactions

R. Bruce Martin, Regina I. Hedrick, Alice Parcell

pp 3197–3206

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a018

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Fused-Ring Systems Containing 1,2,4-Benzothiadiazines. I. The Reaction of o-Aminobenzenesulfonamides with Dibasic Acid Anhydrides

Stanley C. Bell, Peter H. L. Wei, Scott J. Childress

pp 3206–3209

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a019

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Studies on the Thiation of Purines¹

Alfredo Giner-Sorolla, Edna Thom, Aaron Bendich

pp 3209–3212

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a020

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Synthesis of a Renin Substrate

Robert H. Mazur, James M. Schlatter

pp 3212–3216

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a021

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Reactions of Metal Chelates. VII. Dimethylaminomethylation and Chloromethylation of Metal Acetylacetonates¹

Robert H. Barker, James P. Collman, Roger L. Marshall

pp 3216–3220

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a022

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Synthesis of Triaryltin Hydrides^1,2

Alfred Stern, Ernest I. Becker

pp 3221–3225

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a023

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The Preparation and Stabilization of Acetylenic Boranes^1a

E. C. Ashby, W. E. Foster

pp 3225–3229

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a024

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Arylboronic Acids. VIII. Reactions of Boronophthalide¹

R. R. Haynes, H. R. Snyder

pp 3229–3233

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a025

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Organometallic Chemistry. VII. The Reactions of Amylsodium with Norbornene, endo-5-Hydroxymethylnorbornene, Nortricyclene, and Norbornadiene^1,2

Richard A. Finnegan, Robert S. McNees

pp 3234–3241

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a026

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Organometallic Chemistry. VIII. The Metalation of Camphene, Norcamphene, and α-Pinene^1,2

Richard A. Finnegan, Robert S. McNees

pp 3241–3245

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a027

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Paracyclophanes. III. Octamethyl[2.2]paracyclophane. A Highly Strained Cyclophane¹

Daniel T. Longone, Lydia H. Simanyi

pp 3245–3249

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a028

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Condensations at the Methyl Group of Ethyl Acetoacetate by Means of Potassium Amide or Sodium Hydride¹

James F. Wolfe, Thomas M. Harris, Charles R. Hauser

pp 3249–3252

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a029

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An Unusual Reaction Product from Epichlorohydrin and Sodium Cyanide

Francis Johnson, J. P. Heeschen

pp 3252–3258

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a030

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Mechanism of the Desulfurization of Episulfides with Methyl Iodide¹

George K. Helmkamp, David J. Pettitt

pp 3258–3262

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a031

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The Mechanism of Dimethyl Sulfoxide Catalysis in Nucleophilic Displacement

Charles A. Kingsbury

pp 3262–3270

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a032

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The Reaction of Phenyllithium with Some Dialkyl and 1,2-Alkylene Sulfates

Kenneth K. Andersen, Stuart W. Fenton

pp 3270–3273

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a033

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Grignard Reagents of Sulfones. VIII. Reactions of Alkylene Disulfones with Ethylmagnesium Bromide¹

Lamar Field, Edwin T. Boyd

pp 3273–3276

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a034

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Reaction of Dimethylsulfonium Methylide with Vinylic Sulfones. Formation of Aryl Cyclopropyl Sulfones

William E. Truce, Virupax V. Badiger

pp 3277–3280

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a035

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Halogen and Nucleoside Derivatives of Acyclic 2-Amino-2-deoxy-D-glucose.^1,2 I

M. L. Wolfrom, H. G. Garg, D. Horton

pp 3280–3283

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a036

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Synthetic Confirmation of an Interglycosidic Linkage in Heparin¹

M. L. Wolfrom, H. El Khadem, J. R. Vercellotti

pp 3284–3286

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a037

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Synthesis of the Two 2-O-Nitro-3,5-di-O-p-nitrobenzoyl-D-arabinofuranosyl Chlorides, an Anomeric Pair of Crystalline Pentofuranosyl Halides Having a Nonparticipating Group at C-2

C. P. J. Glaudemans, Hewitt G. Fletcher Jr.

pp 3286–3290

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a038

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Preparation and Hydrolysis of Methyl 1-Thio-β-D-xylothiopyranoside¹

Roy L. Whistler, R. M. Rowell

pp 3290–3291

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a039

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Homogeneous Hydrogenation of Methyl Linoleate Catalyzed by Iron Pentacarbonyl. Characterization of Methyl Octadecadienoate—Iron Tricarbonyl Complexes¹

E. N. Frankel, E. A. Emken, Helen M. Peters, V. L. Davison, R. O. Butterfield

pp 3292–3297

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a040

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Synthesis and Ozonolysis of Benzo[c]phenanthrene^1-3

Emil J. Moriconi, Ludwig Salce, Lubomyr B. Taranko

pp 3297–3299

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a041

First Page

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Steroids. CCLXV.¹ Studies in Cyano Steroids. III.² Unsaturated 2-Cyano Steroids

James C. Orr, Arcelia de la Roz, A. Bowers

pp 3300–3303

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a042

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Conformational Analysis of Steroidal 16,17-Diketones

Leland J. Chinn

pp 3304–3305

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a043

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The Addition of Ketones to Schiff Bases

A. H. Blatt, Norma Gross

pp 3306–3311

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a044

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Rotatory Dispersion Studies. IV.^1a Substituted Cyclohexanone Oximes^1b

Gloria G. Lyle, Renée Mestrallet Barrera

pp 3311–3314

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a045

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The Synthesis of Some Compounds Related to 3-Amino-1-propanethiol¹

D. S. Tarbell, David A. Buckley, Paula Pimlott Brownlee, Ralph Thomas, James S. Todd

pp 3314–3319

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a046

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A Chlorinative Ring Expansion. The Reaction of t-Butyl Hypochlorite and 1-Vinylcycloalkanols¹

Carl R. Johnson, Clair J. Cheer, David J. Goldsmith

pp 3320–3323

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a047

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Synthesis of Oximes¹

Sylvan E. Forman

pp 3323–3327

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a048

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The Chemistry of Carbanions. VI. Stereochemistry of the Wittig Reaction with Stabilized Ylids^1a

Herbert O. House, Vera K. Jones, George A. Frank

pp 3327–3333

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a049

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Transformation Products of the Photoadduct of p-Xylene and Phenanthrenequinone. Some Two- and Three-Atom Bridged Biphenyls¹

Mordecai B. Rubin

pp 3333–3340

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a050

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Generation of Methyl Radicals by Decomposition of Bibenzyl Compounds Containing α-Methoxy Substituents

G. E. Hartzell, E. S. Huyser

pp 3341–3344

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a051

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The Dehydrochlorination of Allophanoyl Chlorides. A New Synthesis of Isocyanates

A. A. R. Sayigh, James N. Tilley, Henri Ulrich

pp 3344–3347

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a052

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Some Reactions of Ethylene Diisocyanate

James N. Tilley, A. A. R. Sayigh

pp 3347–3350

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a053

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Conversion of a 1,2-Glycol Monocarbamate into Two Isomeric 1-Piperidinecarboxylates

Antonio Da Settimo, Marco F. Saettone

pp 3350–3353

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a054

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Some Observations on Allylic Oxidation¹

Kenneth B. Wiberg, Stuart D. Nielsen

pp 3353–3361

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a055

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A Synthesis of Iridomyrmecin

Keiiti Sisido, Kiitiró Utimoto, Tyûzô Isida

pp 3361–3365

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a056

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Intramolecular Nucleophilic Participation. IV. The Hydrolysis Rates of Various ortho- and para-Substituted 1,1-Diphenylethyl Chlorides and Benzhydryl Chlorides and Bromides in Aqueous Acetone

E. A. Jeffery, R. K. Bansal, L. J. Andrews, R. M. Keefer

pp 3365–3370

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a057

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Nucleophilic Displacement Reactions of 2-Amino-4-alkylthiopteridines^1-3

John J. McCormack, Henry G. Mautner

pp 3370–3373

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a058

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Photochemistry of Stilbenes. IV. The Preparation of Substituted Phenanthrenes^1a-c

Clelia S. Wood, Frank B. Mallory

pp 3373–3377

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a059

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A Preparation of β-Sitosterol^1a

G. I. Fujimoto, A. E. Jacobson

pp 3377–3381

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a060

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The Reaction between 4-Nitroquinoline 1-Oxide and Diethyl Sodiomalonate. An Unexpected Nucleophilic Substitution¹

Henry J. Richter, Norman E. Rustad

pp 3381–3383

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a061

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Small Charged Rings. V. Expansion of the Aziridinium Ring by Reaction with Ketones^1-4

Nelson J. Leonard, Joseph V. Paukstelis, Leonard E. Brady

pp 3383–3386

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a062

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The Nitration of Toluene with Alkyl Nitrates and Polyphosphoric Acid¹

S. M. Tsang, A. P. Paul, M. P. DiGiaimo

pp 3387–3390

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a063

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The Chlorination of Reactive Anilines

R. S. Neale, R. G. Schepers, M. R. Walsh

pp 3390–3393

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a064

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The Configurational Relationships of the cis-β-Decalols and cis-β-Decalylamines¹

Theodore Cohen, M. Malaiyandi, Jack L. Pinkus

pp 3393–3396

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a065

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Notes

pp 3396–3452

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a066

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Deiodination of Iodophenyl Phenyl Ethers with Hydriodic Acid^1,2

Eugene C. Jorgensen, James A. W. Reid

pp 3396–3398

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a501

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Chlorination of Methaneboronic Acid Derivatives with t-Butyl Hypochlorite

Donald S. Matteson

pp 3399–3400

Publication Date: November 1964 (Article)

DOI: 10.1021/jo01034a502

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The Structure and Some Properties of Phenylhydrazine Borane and 1,1-Diphenylhydrazine Borane

Ronald J. Baumgarten, Malcolm C. Henry

pp 3400–3403

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a503

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The Preparation of 2-Arylimidazo[4,5-b]pyridines

D. L. Garmaise, J. Komlossy

pp 3403–3405

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a504

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Organoboron Compounds. XVIII. Bifunctional Binding of Water by the cis-1,2-Cyclopentanediol Ester of 8-Quinolineboronic Acid

James D. Morrison, R. L. Letsinger

pp 3405–3407

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a505

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A Synthesis of 1,2,3,4,6,7,12,12b-Octahydro-2-oxoindolo[2,3-a] quinolizine¹

K. T. Potts, I. D. Nasri

pp 3407–3410

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a506

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Synthesis of 5-Alkyl-5,10-dihydro-10-phenylphenophosphazine

George Baum, Helen A. Lloyd, Christ Tamborski

pp 3410–3411

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a507

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The Equilibrium Protonation and Acid-Catalyzed Detritiation of Cycl[3.2.2]azine¹

Robert J. Thomas, F. A. Long

pp 3411–3412

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a508

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Reactions of Triphenylphosphinalkylimines with Boron Trifluoride¹

Hans Zimmer, Gurdial Singh

pp 3412–3414

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a509

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The Reaction of Silver 2-Bromo-3-methyl-2-butenoate with 1,1-Diphenylethylene

H. D. Hartzler

pp 3414–3415

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a510

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Separation and Determination of the Hydrolysis Products of a Methylated Xylan as Their Trimethylsilyl Derivatives by Vapor Phase Chromatography

Hugo H. Sephton

pp 3415–3416

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a511

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3-Hydroxymethyl-1-(5-nitrofurfurylideneamino)hydantoin¹

Claude F. Spencer, Julian G. Michels

pp 3416–3418

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a512

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The Preparation of Some α,ι-Dichloro Permethylated Polysilanes

Henry Gilman, Shohei Inoue

pp 3418–3419

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a513

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Ozonolysis of Certain Acetylenic Alcohols¹

Joseph G. Cannon, Laszlo L. Darko

pp 3419–3420

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a514

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Photoinduced Condensations of Nitroaromatics

Virgil I. Stenberg, Dwight J. Holter

pp 3420–3422

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a515

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Formic Ethylcarbonic Anhydride¹

T. Parasaran, D. S. Tarbell

pp 3422–3423

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a516

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A Convenient Preparation of 1-Diazopropane

John R. Dyer, R. B. Randall Jr., Howard M. Deutsch

pp 3423–3424

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a517

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Formation of 1,3-Dioxanes in Water

F. R. Galiano, D. Rankin, G. J. Mantell

pp 3424–3426

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a518

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A Re-examination of the Conformational Analysis of the Tropine-Pseudotropine System¹

Herbert S. Aaron, Charles P. Rader

pp 3426–3427

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a519

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A Study of the Rhodium Catalyzed Hydrogenation of 1-Naphthol. An Improved Preparation of 1- and 2-Decalols¹

A. I. Meyers, W. Beverung, G. Garcia-Munoz

pp 3427–3429

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a520

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Reaction of a Schiff Base with Nitrogen Tetroxide. A Novel Synthesis of an Anhydrous Diazonium Salt

Richard M. Scribner

pp 3429–3430

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a521

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Ferrocenes. VII. Ferrocenes from Monofunctional Cyclopentadienes

Robert L. Schaaf, Carl T. Lenk

pp 3430–3433

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a522

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Pyrolytic Conversion of 7,7-Dichloronorcarane to Cycloheptatriene

G. C. Robinson

pp 3433–3434

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a523

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The Synthesis of 2,3,6-Tri-O-methyl-D-galactose and Its Derivatives¹

Neil R. Williams, Roger W. Jeanloz

pp 3434–3436

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a524

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The Synthesis of Homoribose¹

John A. Montgomery, Kathleen Hewson

pp 3436–3438

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a525

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Constituents of Ambrosia hispida Pursh.^1,2

Werner Herz, Yasuo Sumi

pp 3438–3439

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a526

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Inclusion Compounds of Carbohydrates and Related Compounds¹

Harmon L. Hoffman Jr., George R. Breeden Jr., R. Winston Liggett

pp 3440–3441

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a527

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Studies on the Alkaloids of Securinega virosa Pax. et Hoffm. IV.¹ The Preferred Conformations of Allosecurinine (Phyllochrysine) and Dihydrosecurinine

T. Nakano, T. H. Yang, S. Terao

pp 3441–3443

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a528

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The Tritiation of Diethyl Benzylacetamidomalonate by Exposure to Tritium Gas

Helen Krizek, Anthony J. Verbiscar, Weldon G. Brown

pp 3443–3445

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a529

First Page

Hi-Res PDF[442K]

Two Abbreviated Syntheses of Flavones and Flavone Analogs

L. L. Woods, John Sapp

pp 3445–3447

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a530

First Page

Hi-Res PDF[364K]

Some Diels—Alder Studies of the 1,3-Dihydro-2H-azepin-2-ones¹

Leo A. Paquette

pp 3447–3449

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a531

First Page

Hi-Res PDF[413K]

The Diazotization and Autocoupling of Guanazole¹

M. Hauser

pp 3449–3450

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a532

First Page

Hi-Res PDF[282K]

Some Merocyanines with Chelating Properties

J. W. Faller, A. Mueller, J. P. Phillips

pp 3450–3452

Publication Date: November 1964 ()

DOI: 10.1021/jo01034a533

First Page

Hi-Res PDF[383K]

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