Articles ASAP (As Soon As Publishable)

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February 9, 2010

Flow Processing of Microwave-Assisted (Heterogeneous) Organic Reactions

Mark H. C. L. Dressen, Bastiaan H. P. van de Kruijs, Jan Meuldijk, Jef A. J. M. Vekemans and Lumbertus A. Hulshof
Publication Date (Web): February 9, 2010 (Article)
DOI: 10.1021/op900257f

February 4, 2010

Nonchromatographic Isolation of 2-Alkyl-2H-1,2,3-Triazoles in the Synthesis of NK3 Receptor Antagonists

Huan Wang and Hao Yin
Publication Date (Web): February 4, 2010 (Technical Note)
DOI: 10.1021/op900320j

A Synthesis of 3,5-Disubstituted Phenols

James P. Davidson, Keshab Sarma, Dan Fishlock, Michael H. Welch, Sunil Sukhtankar, Gary M. Lee, Michael Martin and Gary F. Cooper
Publication Date (Web): February 4, 2010 (Technical Note)
DOI: 10.1021/op900322u

February 1, 2010

ReactIR Flow Cell: A New Analytical Tool for Continuous Flow Chemical Processing

Catherine F. Carter, Heiko Lange, Steven V. Ley, Ian R. Baxendale, Brian Wittkamp, Jon G. Goode and Nigel L. Gaunt
Publication Date (Web): February 1, 2010 (Article)
DOI: 10.1021/op900305v

Scaleable Preparation of Functionalized Organometallics via Directed Ortho Metalation Using Mg- and Zn-Amide Bases

Stefan H. Wunderlich, Christoph J. Rohbogner, Andreas Unsinn and Paul Knochel
Publication Date (Web): February 1, 2010 (Article)
DOI: 10.1021/op9002888

January 29, 2010

Improved Synthesis of RO4858542, a 5-HT6 Receptor Antagonist

Qingwu Jin, Michael Welch and Lawrence Fisher
Publication Date (Web): January 29, 2010 (Technical Note)
DOI: 10.1021/op900319p

Continuous Acid-Catalyzed Methylations in Supercritical Carbon Dioxide: Comparison of Methanol, Dimethyl Ether and Dimethyl Carbonate as Methylating Agents

Peter N. Gooden, Richard A. Bourne, Andrew J. Parrott, Han S. Bevinakatti, Derek J. Irvine and Martyn Poliakoff
Publication Date (Web): January 29, 2010 (Article)
DOI: 10.1021/op900307w

January 28, 2010

Photodimerization of Maleic Anhydride in a Microreactor Without Clogging

Tomoaki Horie, Motoshige Sumino, Takumi Tanaka, Yoshihisa Matsushita, Teijiro Ichimura and Jun-ichi Yoshida
Publication Date (Web): January 28, 2010 (Article)
DOI: 10.1021/op900306z

January 26, 2010

Aminolysis of Epoxides in a Microreactor System: A Continuous Flow Approach to β-Amino Alcohols

Matthew W. Bedore, Nikolay Zaborenko, Klavs F. Jensen and Timothy F. Jamison
Publication Date (Web): January 26, 2010 (Article)
DOI: 10.1021/op9003136

A Practical Synthesis of Regioisomeric 6- and 7-Methoxytetrahydro-3-benzazepines

Jimmy T. Liang, Jing Liu, Brock T. Shireman, Vi Tran, Xiaohu Deng and Neelakandha S. Mani
Publication Date (Web): January 26, 2010 (Article)
DOI: 10.1021/op900292j

In Situ FTIR Study and Scale-Up of An Enolization−Azidation Sequence

Terrence J. Connolly, Eric C. Hansen and Michael F. MacEwan
Publication Date (Web): January 26, 2010 (Communication to Editor)
DOI: 10.1021/op900299c

January 15, 2010

Synthesis and Process Optimization of Amtolmetin: An Antiinflammatory Agent

Lekkala Amarnath Reddy, Saurya Chakraborty, Rodda Swapna, Dinesh Bhalerao, Golla China Malakondaiah, Mylavarapu Ravikumar, Abhijeet Kumar, Gade Srinivas Reddy, Jyothirmayi Naram, Namrata Dwivedi, Arnab Roy, Vurimidi Himabindu, Bangaru Babu, Apurba Bhattacharya and Rakeshwar Bandichhor
Publication Date (Web): January 15, 2010 (Article)
DOI: 10.1021/op900284w

January 7, 2010

Green Chemistry: Cresting a Summit toward Sustainability

John L. Tucker
Publication Date (Web): January 7, 2010 (Concept Article)
DOI: 10.1021/op9000548

January 5, 2010

A New Method for Synthesis of Nolatrexed Dihydrochloride

Xueqing Zhao, Fei Li, Weiping Zhuang, Xiaowen Xue, Yuanyang Lian, Jianhui Fan and Dongsheng Fang
Publication Date (Web): January 5, 2010 (Article)
DOI: 10.1021/op9002517

November 6, 2009

Application of Quality by Design Principles to Support Development of a Control Strategy for the Control of Genotoxic Impurities in the Manufacturing Process of a Drug Substance

Zadeo Cimarosti, Fernando Bravo, Paul Stonestreet, Francesco Tinazzi, Orsola Vecchi and Giulio Camurri
Publication Date (Web): November 6, 2009 (Article)
DOI: 10.1021/op900242x
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