Table of Contents

Journal Cover
November 18, 1999
Volume 1, Issue 10
Pages 1505-1687
For Selected Content:

Letters

One-Pot Synthesis of Pyrroles through Carbometalation Reaction of Zincated Hydrazone with Vinylstannane

Masaharu Nakamura, Kenji Hara, Go Sakata, and Eiichi Nakamura
pp 1505–1507
Publication Date (Web): October 20, 1999 (Letter)
DOI: 10.1021/ol990911h

Novel Metal-Free Bis-silylation:  C60-Sensitized Reaction of Disilirane with Benzonitrile

Takeshi Akasaka, Yutaka Maeda, Takatsugu Wakahara, Mutsuo Okamura, Mamoru Fujitsuka, Osamu Ito, Kaoru Kobayashi, Shigeru Nagase, Masahiro Kako, Yasuhiro Nakadaira, and Ernst Horn
pp 1509–1512
Publication Date (Web): October 07, 1999 (Letter)
DOI: 10.1021/ol9901772

Aminoethylprolyl Peptide Nucleic Acids (aepPNA):  Chiral PNA Analogues That Form Highly Stable DNA:aepPNA2 Triplexes

Moneesha D'Costa, Vaijayanti A. Kumar, and Krishna N. Ganesh
pp 1513–1516
Publication Date (Web): October 15, 1999 (Letter)
DOI: 10.1021/ol990835i

Efficient Synthesis of 2-Deoxy l-Ribose from l-Arabinose:  Mechanistic Information on the 1,2-Acyloxy Shift in Alkyl Radicals

Michael E. Jung and Yue Xu
pp 1517–1519
Publication Date (Web): October 06, 1999 (Letter)
DOI: 10.1021/ol990838v

Cathodic Reduction of Phenacyl Azides

Belén Batanero, José Escudero, and Fructuoso Barba
pp 1521–1522
Publication Date (Web): October 20, 1999 (Letter)
DOI: 10.1021/ol990200j

Convergent Synthesis of p-Benzylcalix[7]arene:  Condensation and UHIG of p-Benzylcalix[6 or 8]arenes

Jerry L. Atwood, Michaele J. Hardie, Colin L. Raston, and Christian A. Sandoval
pp 1523–1526
Publication Date (Web): October 28, 1999 (Letter)
DOI: 10.1021/ol9908272

Promiscuous Watson−Crick Cross-Pairing within the Family of Pentopyranosyl (4‘→2‘) Oligonucleotides1

Oliver Jungmann, Harald Wippo, Michael Stanek, Hoan K. Huynh, Ramanarayanan Krishnamurthy, and Albert Eschenmoser
pp 1527–1530
Publication Date (Web): October 22, 1999 (Letter)
DOI: 10.1021/ol990183y

l-α-Lyxopyranosyl (4‘→3‘) Oligonucleotides:  A Base-Pairing System Containing a Shortened Backbone1

Folkert Reck, Harald Wippo, René Kudick, Martin Bolli, Griet Ceulemans, Ramanarayanan Krishnamurthy, and Albert Eschenmoser
pp 1531–1534
Publication Date (Web): October 22, 1999 (Letter)
DOI: 10.1021/ol990184q

Studies on Inducers of Nerve Growth Factor:  Synthesis of the Cyathin Core

Dennis L. Wright, Christopher R. Whitehead, E. Hampton Sessions, Ion Ghiviriga, and Dean A. Frey
pp 1535–1538
Publication Date (Web): October 24, 1999 (Letter)
DOI: 10.1021/ol991032y

Thia-Wittig-like Reactions as a New Route for the Stereoselective Synthesis of (Z)-Fluoroalkenoates

David Chevrie, Thierry Lequeux, and Jean-Claude Pommelet
pp 1539–1541
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol990178u

The Use of High-Resolution NMR Spectroscopy in Supramolecular Systems

Peter Forgo and Valerian T. D'Souza
pp 1543–1545
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol990848w

β-Siloxy Unsaturated Nitriles:  Stereoselective Cyclizations to cis- and trans-Decalins

Fraser F. Fleming, Brian C. Shook, Tao Jiang, and Omar W. Steward
pp 1547–1550
Publication Date (Web): October 14, 1999 (Letter)
DOI: 10.1021/ol990854s

Synthesis of Isoindolo[2,1-a]indoles by the Palladium-Catalyzed Annulation of Internal Alkynes

Kevin R. Roesch and Richard C. Larock
pp 1551–1553
Publication Date (Web): October 07, 1999 (Letter)
DOI: 10.1021/ol9901873

Synthesis of Hexabenzotriphenylene and Other Strained Polycyclic Aromatic Hydrocarbons by Palladium-Catalyzed Cyclotrimerization of Arynes

Diego Peña, Dolores Pérez, Enrique Guitián, and Luis Castedo
pp 1555–1557
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol990864t

Methylsulfenylation of Thioacetals as a Method for Synthesizing 2-Thio-Substituted Furans

Albert Padwa, John D. Ginn, and Michael S. McClure
pp 1559–1561
Publication Date (Web): October 06, 1999 (Letter)
DOI: 10.1021/ol990865l

Enantioselective Palladium-Catalyzed Allylic Alkylation Using E- and Z-Vinylogous Sulfonates

P. Andrew Evans and Thomas A. Brandt
pp 1563–1565
Publication Date (Web): October 16, 1999 (Letter)
DOI: 10.1021/ol990879r

Stereoselective 1,4-Silaboration of 1,3-Dienes Catalyzed by Nickel Complexes

Michinori Suginome, Takanori Matsuda, Takayo Yoshimoto, and Yoshihiko Ito
pp 1567–1569
Publication Date (Web): October 19, 1999 (Letter)
DOI: 10.1021/ol990908y

(R)- and (S)-3-Fluorothalidomides:  Isosteric Analogues of Thalidomide

Yoshio Takeuchi, Tomoki Shiragami, Kenichi Kimura, Emiko Suzuki, and Norio Shibata
pp 1571–1573
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol9902172

New Two-Photon Absorbing Fluorene Derivatives:  Synthesis and Nonlinear Optical Characterization

Kevin D. Belfield, David J. Hagan, Eric W. Van Stryland, Katherine J. Schafer, and Raluca A. Negres
pp 1575–1578
Publication Date (Web): October 06, 1999 (Letter)
DOI: 10.1021/ol9909177

Synthesis of Nitrogen Heterocycles by Intramolecular Michael Type of Amination via Reduction of Imines with Di-n-butyliodotin Hydride (n-Bu2SnIH)

Toshihiro Suwa, Ikuya Shibata, Keita Nishino, and Akio Baba
pp 1579–1581
Publication Date (Web): October 15, 1999 (Letter)
DOI: 10.1021/ol990225i

Double Annulation Route to Fused Bicyclic Compounds with Three Contiguous Quaternary Centers

Robert B. Grossman, Aaron J. Skaggs, Arlene E. Kray, and Brian O. Patrick
pp 1583–1586
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol990935o

Five-Membered-Ring 9-I-2 Radicals:  Direct Detection and Comparison with Other Hypervalent Iodine Radicals

Miguel A. Miranda, Julia Pérez-Prieto, Enrique Font-Sanchis, and J. C. Scaiano
pp 1587–1589
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol990229n

Reaction of Silyl Enol Ethers with Xenon Difluoride in MeCN:  Evidence for a Nonclassical Radical Cation Intermediate

Christopher A. Ramsden and Rachel G. Smith
pp 1591–1594
Publication Date (Web): October 06, 1999 (Letter)
DOI: 10.1021/ol990231e

Highly Diastereoselective Reaction of 2-Azanorbornyl Enolates with Electrophiles

Diego A. Alonso, Sofia J. M. Nordin, and Pher G. Andersson
pp 1595–1597
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol990942c

Stereoselective, Oxidative C−C Bond Coupling of Naphthopyran Induced by DDQ:  Stereocontrolled Total Synthesis of Deoxyfrenolicin

Yao-Chang Xu, Dan T. Kohlman, Sidney X. Liang, and Chad Erikkson
pp 1599–1602
Publication Date (Web): October 09, 1999 (Letter)
DOI: 10.1021/ol9909738

Computational Studies of Oxahalocarbene Fragmentation:  Convergence of Theory and Experiment

Shunqi Yan, Ronald R. Sauers, and Robert A. Moss
pp 1603–1606
Publication Date (Web): October 16, 1999 (Letter)
DOI: 10.1021/ol9902475

Novel Bridged Bicyclic α-Amino Acid Esters and Key Derivatives from Quincorine and Quincoridine

Olaf Schrake, Volker S. Rahn, Jens Frackenpohl, Wilfried M. Braje, and H. Martin R. Hoffmann
pp 1607–1610
Publication Date (Web): November 11, 1999 (Letter)
DOI: 10.1021/ol990981o

Enantioselective Ring Opening of Meso Aziridines Catalyzed by Tridentate Schiff Base Chromium(III) Complexes

Zhen Li, Mónica Fernández, and Eric N. Jacobsen
pp 1611–1613
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol990992h

Facile Autoxidation of 2-(4-Hydroxy- phenyl)-3,3-dimethylmethylenecyclopropane. The Radical Stabilizing Ability of the Phenoxide Group

Xavier Creary, Allison Wolf, and Kevin Miller
pp 1615–1618
Publication Date (Web): October 09, 1999 (Letter)
DOI: 10.1021/ol9902576

A Simple Synthesis of 2-Substituted-4H-3,1-benzoxazin-4-ones by Palladium-Catalyzed Cyclocarbonylation of o-Iodoanilines with Acid Chlorides

Chitchamai Larksarp and Howard Alper
pp 1619–1622
Publication Date (Web): October 07, 1999 (Letter)
DOI: 10.1021/ol990258y

Sets of Aldolase Antibodies with Antipodal Reactivities. Formal Synthesis of Epothilone E by Large-Scale Antibody-Catalyzed Resolution of Thiazole Aldol

Subhash C. Sinha, Jian Sun, Gregory Miller, Carlos F. Barbas, III, and Richard A. Lerner
pp 1623–1626
Publication Date (Web): October 16, 1999 (Letter)
DOI: 10.1021/ol990261h

First Total Synthesis of (±)-Methyl Gummiferolate Using a Homoallyl−Homoallyl Radical Rearrangement Reaction

Masahiro Toyota, Masahiro Yokota, and Masataka Ihara
pp 1627–1629
Publication Date (Web): October 15, 1999 (Letter)
DOI: 10.1021/ol990264u

Intramolecular Reactivity of a Captodative Bis-Diene

Silvia Aime, Hassan Oulyadi, Jacques Maddaluno, and Paolo Venturello
pp 1631–1634
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol991000a

Ruthenium-Catalyzed Regioselective Codimerization of Enol Acylates with 2-Substituted-1,3-butadienes

Mitsuhiko Fujiwhara, Takenobu Nishikawa, and Yoji Hori
pp 1635–1637
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol991004f

Nitroazole Universal Bases in Peptide Nucleic Acids

Hemavathi Challa, Melanie L. Styers, and Stephen A. Woski
pp 1639–1641
Publication Date (Web): September 29, 1999 (Letter)
DOI: 10.1021/ol990270q

Titanium(IV) Triflates in the Catalysis of Homoaldol Reactions

Evelyn O. Martins and James L. Gleason
pp 1643–1645
Publication Date (Web): October 15, 1999 (Letter)
DOI: 10.1021/ol991017t

The N-Acyliminium Pictet−Spengler Condensation as a Multicomponent Combinatorial Reaction on Solid Phase and Its Application to the Synthesis of Demethoxyfumitremorgin C Analogues

Haishan Wang and A. Ganesan
pp 1647–1649
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol991030d

Oxidized Arenol Intermediates in Intermolecular Carbon−Carbon Bond Formation. Naphthoid Cyclohexa-2,4-dienones via Oxidative Nucleophilic Substitution

Stéphane Quideau, Matthew A. Looney, and Laurent Pouységu
pp 1651–1654
Publication Date (Web): October 17, 1999 (Letter)
DOI: 10.1021/ol9910363

Metabolism of the Host-Selective Toxins Destruxin B and Homodestruxin B:  Probing a Plant Disease Resistance Trait

M. Soledade C. Pedras, Irina. L. Zaharia, Yuanzhu Gai, Kevin C. Smith, and Dale E. Ward
pp 1655–1658
Publication Date (Web): October 20, 1999 (Letter)
DOI: 10.1021/ol991042z

Facile Synthesis of Substituted Phenanthroline Ligands by Samarium-Promoted Coupling of Phenanthroline with Ketones

David J. O'Neill and Paul Helquist
pp 1659–1662
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol990284w

Efficient Synthesis of a Novel 4-Hydroxy-2,3-dioxocyclobut-1-enyl Group Containing Amino Acids

Tetsuro Shinada, Ken-ichi Hayashi, Toshihiro Hayashi, Yasutaka Yoshida, Manabu Horikawa, Keiko Shimamoto, Yasushi Shigeri, Noboru Yumoto, and Yasufumi Ohfune
pp 1663–1666
Publication Date (Web): October 15, 1999 (Letter)
DOI: 10.1021/ol990286g

Enantiomerically Pure trans-3,4-Disubstituted Tetrahydrothiophenes from Diastereoselective Thiocarbonyl Ylide Addition to Chiral α,β-Unsaturated Amides

Staffan Karlsson and Hans-Erik Högberg
pp 1667–1669
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol9910565

First Total Synthesis of Xestobergsterol A and Active Structural Analogues of the Xestobergsterols1

Michael E. Jung and Ted W. Johnson
pp 1671–1674
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol991057x

Distinguishing the SN2 and the SN2‘ Mechanisms in the Gas Phase

Gustavo E. Davico
pp 1675–1678
Publication Date (Web): October 07, 1999 (Letter)
DOI: 10.1021/ol990290s

Synthesis of a Novel Chiral Binaphthyl Phospholane and Its Application in the Highly Enantioselective Hydrogenation of Enamides

Dengming Xiao, Zhaoguo Zhang, and Xumu Zhang
pp 1679–1681
Publication Date (Web): October 20, 1999 (Letter)
DOI: 10.1021/ol991074m

Potassium Alkenyl- and Aryltrifluoroborates:  Stable and Efficient Agents for Rhodium-Catalyzed Addition to Aldehydes and Enones

Robert A. Batey, Avinash N. Thadani, and David V. Smil
pp 1683–1686
Publication Date (Web): October 10, 1999 (Letter)
DOI: 10.1021/ol9910767

Additions and Corrections

Carbon−Carbon Bond Formation via Palladium-Catalyzed Reductive Coupling in Air

Sripathy Venkatraman and Chao-Jun Li
p 1687
Publication Date (Web): October 16, 1999 (Additions & Corrections)
DOI: 10.1021/ol991094o

A Novel Safety-Catch Linker for the Solid-Phase Synthesis of Amides and Esters

Matthew H. Todd, Steven F. Oliver, and Chris Abell
p 1687
Publication Date (Web): October 16, 1999 (Additions & Corrections)
DOI: 10.1021/ol991109i
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