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Growth of Boron-Doped Diamond Films on Gold-Coated Substrates with and without Gold Nanoparticle Formation

  • Shannon S. Nicley*
    Shannon S. Nicley
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
    Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, United Kingdom
    *E-mail: [email protected]
  • Sien Drijkoningen
    Sien Drijkoningen
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
  • Paulius Pobedinskas
    Paulius Pobedinskas
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
  • Jorne Raymakers
    Jorne Raymakers
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
  • Wouter Maes
    Wouter Maes
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
    More by Wouter Maes
  • , and 
  • Ken Haenen
    Ken Haenen
    Institute for Materials Research, Hasselt University, and IMOMEC, IMEC vzw, Wetenschapspark 1, 3590 Diepenbeek, Belgium
    More by Ken Haenen
Cite this: Cryst. Growth Des. 2019, 19, 6, 3567–3575
Publication Date (Web):May 1, 2019
https://doi.org/10.1021/acs.cgd.9b00488
Copyright © 2019 American Chemical Society

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    Abstract

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    This work describes the growth of boron-doped nanocrystalline diamond (B:NCD) films on gold-coated substrates and methodologies for achieving B:NCD with either smooth morphologies or on top of gold nanoparticles (AuNPs) of varying sizes controlled by the surface pretreatment. B:NCD is deposited uniformly over ∼1 cm2 gold-coated substrates. AuNPs of ∼100–500 nm diameter formed during microwave plasma-assisted chemical vapor deposition, and these were overgrown by diamond. The size of the AuNPs under the diamond film can be increased by oxygen treatment of the surface prior to growth. AuNPs under the diamond film can be suppressed by growing a diamond nucleation layer at a lower temperature and in the presence of CO2 in a linear antenna diamond growth reactor.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.cgd.9b00488.

    • EDX spectroscopy results of faceted gold nanoparticles at the edge of gold coated region, as described in the text (PDF)

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    Cited By

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