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Fine Tuning the Heterostructured Interfaces by Topological Transformation of Layered Double Hydroxide Nanosheets

  • Yanqi Xu
    Yanqi Xu
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029 People’s Republic of China
    More by Yanqi Xu
  • , 
  • Zelin Wang
    Zelin Wang
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029 People’s Republic of China
    More by Zelin Wang
  • , 
  • Ling Tan
    Ling Tan
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029 People’s Republic of China
    More by Ling Tan
  • , 
  • Yufei Zhao*
    Yufei Zhao
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029 People’s Republic of China
    *E-mail: [email protected]
    More by Yufei Zhao
    Orcidhttp://orcid.org/0000-0002-5325-8991
  • , 
  • Haohong Duan*
    Haohong Duan
    Department of Chemistry, University of Oxford, 12 Mansfield Road, Oxford, OX1 3TA, U.K.
    *E-mail: [email protected]
    More by Haohong Duan
    Orcidhttp://orcid.org/0000-0002-9241-0984
  • , and 
  • Yu-Fei Song*
    Yu-Fei Song
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029 People’s Republic of China
    *E-mail: [email protected] or [email protected]
    More by Yu-Fei Song
Cite this: Ind. Eng. Chem. Res. 2018, 57, 31, 10411–10420
Publication Date (Web):July 5, 2018
https://doi.org/10.1021/acs.iecr.8b02246
Copyright © 2018 American Chemical Society
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Abstract

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Rational design of highly active, stable, and inexpensive catalysts with abundant interfaces can have great potential to increase catalytic performance. Topological transformation of layered double hydroxides (LDHs) to the corresponding mixed metal oxides (MMOs) offers an efficient strategy to achieve such interfaces. However, the formation and conversion of these heterostructured interfaces is lacking in study and remains elusive. Herein, we report a detailed investigation of the topological transformation of LDHs. The as-prepared MMO with abundant interfaces can be modulated by calcination of ZnCo-LDH at different temperatures. Among them, the ZnCo-LDH calcinated at 200 °C reveals the most abundant interfaces and exhibits excellent performance in electrochemical water oxidation. This work will deepen the understanding of the LDH topological transformation from the molecular level.

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The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.iecr.8b02246.

  • Extended characterization results, including experimental, TG–DTA, XRD, HRTEM, XAFS, XPS, electrocatalysis performance (PDF)

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