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Ligation of Boratabenzene and 9-Borataphenanthrene to Coinage Metals
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    Ligation of Boratabenzene and 9-Borataphenanthrene to Coinage Metals
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    • Greta K. Wisofsky
      Greta K. Wisofsky
      Department of Chemistry and Biochemistry, Baylor University, One Bear Place #97348, Waco, Texas 76798, United States
    • Katherine Rojales
      Katherine Rojales
      Department of Chemistry and Biochemistry, Baylor University, One Bear Place #97348, Waco, Texas 76798, United States
    • Xiaojun Su
      Xiaojun Su
      Department of Chemistry and Biochemistry, Baylor University, One Bear Place #97348, Waco, Texas 76798, United States
      More by Xiaojun Su
    • Tyler A. Bartholome
      Tyler A. Bartholome
      Department of Chemistry and Biochemistry, Baylor University, One Bear Place #97348, Waco, Texas 76798, United States
    • Andrew Molino
      Andrew Molino
      Department of Chemistry and Physics, La Trobe Institute for Molecular Science, La Trobe University, Melbourne, Victoria, Australia 3086
    • Aishvaryadeep Kaur
      Aishvaryadeep Kaur
      Department of Chemistry and Physics, La Trobe Institute for Molecular Science, La Trobe University, Melbourne, Victoria, Australia 3086
    • David J. D. Wilson
      David J. D. Wilson
      Department of Chemistry and Physics, La Trobe Institute for Molecular Science, La Trobe University, Melbourne, Victoria, Australia 3086
    • Jason L. Dutton
      Jason L. Dutton
      Department of Chemistry and Physics, La Trobe Institute for Molecular Science, La Trobe University, Melbourne, Victoria, Australia 3086
    • Caleb D. Martin*
      Caleb D. Martin
      Department of Chemistry and Biochemistry, Baylor University, One Bear Place #97348, Waco, Texas 76798, United States
      *Email: [email protected]
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    Inorganic Chemistry

    Cite this: Inorg. Chem. 2021, 60, 24, 18981–18989
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    https://doi.org/10.1021/acs.inorgchem.1c02800
    Published December 8, 2021
    Copyright © 2021 American Chemical Society

    Abstract

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    The reactions of boratabenzene and borataphenanthrene anions with group 11 Ph3PMCl reagents furnished η2 coordination complexes, with the exception of the copper boratabenzene species that adopted an η6 mode. The binding of arene ligands to copper in an η6 manner is rare, and altering the ancillary ligand on copper to an N-heterocyclic carbene switched the binding of the boratabenzene to η2, indicating that such ligands are capable of vacating coordination sites. The η2 coordination complexes bind side-on, akin to olefins, via a borataalkene unit, although with the carbon atom much more proximal to the metal center than boron.

    Copyright © 2021 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acs.inorgchem.1c02800.

    • 1H, 13C, and 11B NMR spectra for all new compounds; FT-IR spectra; crystallographic data; computational details; and ligand competition studies (PDF)

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    CCDC 21029052102911 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/data_request/cif, or by emailing [email protected], or by contacting The Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033.

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    Cited By

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    This article is cited by 4 publications.

    1. Abdelhak Lachguar, Iker Del Rosal, Laurent Maron, Erwann Jeanneau, Laurent Veyre, Chloé Thieuleux, Clément Camp. π-Bonding of Group 11 Metals to a Tantalum Alkylidyne Alkyl Complex Promotes Unusual Tautomerism to Bis-alkylidene and CO2 to Ketenyl Transformation. Journal of the American Chemical Society 2024, 146 (27) , 18306-18319. https://doi.org/10.1021/jacs.4c02172
    2. Kimberly K. Hollister, Kelsie E. Wentz, Robert J. Gilliard, Jr.. Redox- and Charge-State Dependent Trends in 5, 6, and 7-Membered Boron Heterocycles: A Neutral Ligand Coordination Chemistry Approach to Boracyclic Cations, Anions, and Radicals. Accounts of Chemical Research 2024, 57 (10) , 1510-1522. https://doi.org/10.1021/acs.accounts.4c00096
    3. Masilamani Tamizmani, John R. Tidwell, Eric W. Reinheimer, Brian M. Lindley, Caleb D. Martin. Triple-Decker Iron and Cobalt Complexes Featuring a Bridging 1,2-Diboratabenzene Ligand. Inorganic Chemistry 2023, 62 (19) , 7150-7154. https://doi.org/10.1021/acs.inorgchem.3c00558
    4. Katherine Rojales, Masilamani Tamizmani, Tyler A. Bartholome, Caleb D. Martin. Assessing the donor ability of boratabenzene and 9-borataphenanthrene anions through metal complexes with carbonyl ligands. Dalton Transactions 2022, 51 (45) , 17216-17223. https://doi.org/10.1039/D2DT02795J

    Inorganic Chemistry

    Cite this: Inorg. Chem. 2021, 60, 24, 18981–18989
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.inorgchem.1c02800
    Published December 8, 2021
    Copyright © 2021 American Chemical Society

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