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Solvent-Free Synthesis of CuO/HKUST-1 Composite and Its Photocatalytic Application

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    Solvent-Free Synthesis of CuO/HKUST-1 Composite and Its Photocatalytic Application
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    • Ming Jin
      Ming Jin
      College of Chemistry and Chemical Engineering, Qufu Normal University, Qufu, Shandong 273165, P. R. China
      More by Ming Jin
    • Xuefeng Qian
      Xuefeng Qian
      Institute of Fiber Based New Energy Materials, The Key Laboratory of Advanced Textile Materials and Manufacturing Technology of Ministry of Education, College of Materials and Textiles, Zhejiang Sci-Tech University, Hangzhou, Zhejiang 310018, P. R. China
      More by Xuefeng Qian
    • Junkuo Gao*
      Junkuo Gao
      Institute of Fiber Based New Energy Materials, The Key Laboratory of Advanced Textile Materials and Manufacturing Technology of Ministry of Education, College of Materials and Textiles, Zhejiang Sci-Tech University, Hangzhou, Zhejiang 310018, P. R. China
      *E-mail: [email protected] (J.G.).
      More by Junkuo Gao
      Orcidhttp://orcid.org/0000-0001-9778-4312
    • Jihua Chen
      Jihua Chen
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
      More by Jihua Chen
    • Dale K. Hensley
      Dale K. Hensley
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
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    • Hoi Chun Ho
      Hoi Chun Ho
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
      More by Hoi Chun Ho
    • Rebecca J. Percoco
      Rebecca J. Percoco
      Department of Biology, Geology, and Physical Sciences, Sul Ross State University, Alpine, Texas 79832, United States
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    • Christopher M. Ritzi
      Christopher M. Ritzi
      Department of Biology, Geology, and Physical Sciences, Sul Ross State University, Alpine, Texas 79832, United States
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    • Yanfeng Yue*
      Yanfeng Yue
      Department of Biology, Geology, and Physical Sciences, Sul Ross State University, Alpine, Texas 79832, United States
      *E-mail: [email protected] (Y.Y.).
      More by Yanfeng Yue
      Orcidhttp://orcid.org/0000-0002-0214-1806
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    Inorganic Chemistry

    Cite this: Inorg. Chem. 2019, 58, 13, 8332–8338
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    https://doi.org/10.1021/acs.inorgchem.9b00362
    Published June 12, 2019
    Copyright © 2019 American Chemical Society
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    Abstract

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    A metal–organic framework (MOF) is one kind of crystalline microporous material and is increasingly used as a host of catalytically active guests. Nanostructured materials supported on MOFs have presented enhanced catalytic activity and stability. Templates or several steps are essential to the synthesis of MOF composites. Simple and effective MOF synthesis methods are still challenging. Nanosized copper oxide particles in MOF composites, described as nanosized CuO@HKUST-1, were prepared by a facile solvent-free reaction. These series of CuO@HKUST-1 composites exhibited excellent photocatalytic activity for production of hydrogen and methylene blue (MB) degradation under visible light. This synthesis method provides an effective way to fabricate MOF-related nanocomposite catalysts.

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    Supporting Information

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.inorgchem.9b00362.

    • Diagrammatic sketch of photoexcited hole–electron pair separation for CuO@HKUST-1-20/12; the band gap value of HKUST-1 and CuO, and Mott–Schottky plot of CuO in 0.5 M Na2SO4 aqueous solution; XRD patterns of CuO@HKUST-1-20/12 after three cycles; thermogravimetric analysis of HKUST-1, CuO@HKUST-1-20/12, and CuO@HKUST-1-20/3 under air flow; the nitrogen sorption isotherm (77 K) of HKUST-1; and the pore size distribution of CuO@HKUST-1-20/3 and CuO@HKUST-1-20/12 (PDF)

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    Cited By

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    This article is cited by 58 publications.

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    Inorganic Chemistry

    Cite this: Inorg. Chem. 2019, 58, 13, 8332–8338
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.inorgchem.9b00362
    Published June 12, 2019
    Copyright © 2019 American Chemical Society
    Request reuse permissions

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