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Fabrication of Microcapsules by the Combination of Biomass Porous Carbon and Polydopamine for Dual Self-Healing Hydrogels

  • Shumin Liu
    Shumin Liu
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Shumin Liu
  • Zhilu Rao
    Zhilu Rao
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Zhilu Rao
  • Ruiyue Wu
    Ruiyue Wu
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Ruiyue Wu
  • Zhixiang Sun
    Zhixiang Sun
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Zhixiang Sun
  • Zhiru Yuan
    Zhiru Yuan
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Zhiru Yuan
  • Liangjiu Bai*
    Liangjiu Bai
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    *Phone: +86 535 6669070. E-mail: [email protected]. (L.B.)
    More by Liangjiu Bai
  • Wenxiang Wang*
    Wenxiang Wang
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    *Phone: +86 535 6669070. E-mail: [email protected]. (W.W.)
  • Huawei Yang
    Huawei Yang
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Huawei Yang
  • , and 
  • Hou Chen
    Hou Chen
    School of Chemistry and Materials Science, Ludong University, Key Laboratory of High Performance and Functional Polymers in the Universities of Shandong Province, Collaborative Innovation Center of Shandong Province for High Performance Fibers and Their Composites, Yantai 264025, China
    More by Hou Chen
Cite this: J. Agric. Food Chem. 2019, 67, 4, 1061–1071
Publication Date (Web):January 7, 2019
https://doi.org/10.1021/acs.jafc.8b06241
Copyright © 2019 American Chemical Society

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    Abstract

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    Artificial development of smart materials from agricultural waste or food residues is particularly desirable for green chemistry. In this paper, dual-network self-healing hydrogels were successfully fabricated by using functional microcapsules. These microcapsules were established by biomass porous carbon (PC) after recycling of apple residues. Glutaraldehyde (GA) as the healing agent was embedded in the porous carbon, and the outer surface was coated with polydopamine (PDA). After the microcapsules were added, modifying guar gum-type hydrogels were successfully obtained with dual self-healing performance by the combination of a healing agent and metal–ligand coordination. The self-healing efficiency was about 89.9% from the tension test, and the fracture strength was measured as 7.68 MPa. These results not only highlight a new idea for the utilization of apple residues but also provide a new method for the preparation of excellent self-healing hydrogels.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.jafc.8b06241.

    • BET nitrogen adsorption–desorption isotherms showing the specific surface area of PC and PC-GA@PDA (Figure S1); TGA curves (Figure S2) and Raman spectra (Figure S3) of PC, PC-GA, and PC-GA@PDA used to characterize the successful preparation of microcapsules (PDF)

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