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Thermophysical Properties of Glycols and Glymes

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CICECO—Aveiro Institute of Materials, Department of Chemistry, University of Aveiro, 3810-193 Aveiro, Portugal
Departamento de Química e Bioquímica, Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa, 1749-016 Lisboa, Portugal
§ Departamento de Química e Bioquímica, Centro de Química Estrutural, Faculdade de Ciências, Universidade de Lisboa, 1749-016 Lisboa, Portugal
*E-mail: [email protected]. Tel.: +351 234 401 507. Fax: +351 234 370 084.
Cite this: J. Chem. Eng. Data 2015, 60, 12, 3721–3737
Publication Date (Web):December 1, 2015
https://doi.org/10.1021/acs.jced.5b00662
Copyright © 2015 American Chemical Society

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    Abstract

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    Experimental data for density, viscosity, refractive index and sound speed of 11 glycols and glymes were measured in the temperature range between (283.15 and 373.15) K and at atmospheric pressure. The compounds evaluated include ethylene glycol (EG), diethylene glycol (DEG), triethylene glycol (TriEG), tetraethylene glycol (TeEG), ethylene glycol ethyl ether (EGEE), diethylene glycol methyl ether (DEGME), diethylene glycol dimethyl ether (DEGDME), diethylene glycol ethyl ether (DEGEE), diethylene glycol diethyl ether (DEGDEE), triethylene glycol dimethyl ether (TriEGDME), and tetraethylene glycol dimethyl ether (TeEGDME). Additionally, derivative properties, such isobaric thermal expansion coefficient and isentropic compressibilities were also estimated and discussed. The compounds evaluated were selected to evaluate the impact of molecular structure changes on their thermophysical properties. Effects like the increase in the number of ethoxy groups, shown to lead to an increase of the density, molar volume, viscosity, and refractive index, or the loss of the hydroxyl groups through the substitution of the hydroxyl groups hydrogen by a methyl or ethyl group, shown to lead to a significant decrease on the density, viscosity, and sound speed, are evaluated and discussed.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.jced.5b00662.

    • Refractive index plots; sound speed plots; experimental density data for the glycols and glymes aqueous solutions; experimental sound speed data for the glycols and glymes aqueous solutions; least squares fitting coefficients of the compound's aqueous solutions densities and sound speed; summary of the literature data available for the density, viscosity and sound speed of the studied compounds; and empirical correlations for the viscosity, refractive index and sound speed experimental data. (PDF)

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