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AminoBODIPY Conjugates for Targeted Drug Delivery Systems and Real-Time Monitoring of Drug Release
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    AminoBODIPY Conjugates for Targeted Drug Delivery Systems and Real-Time Monitoring of Drug Release
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    • Martin Porubský
      Martin Porubský
      Department of Organic Chemistry, Faculty of Science, Palacký University, Tr. 17. Listopadu 12, 771 46 Olomouc, Czech Republic
    • Soňa Gurská
      Soňa Gurská
      Institute of Molecular and Translational Medicine, Faculty of Medicine and Dentistry, Palacký University, Hněvotínská 5, 779 00 Olomouc, Czech Republic
    • Jarmila Stanková
      Jarmila Stanková
      Institute of Molecular and Translational Medicine, Faculty of Medicine and Dentistry, Palacký University, Hněvotínská 5, 779 00 Olomouc, Czech Republic
    • Marián Hajdúch
      Marián Hajdúch
      Institute of Molecular and Translational Medicine, Faculty of Medicine and Dentistry, Palacký University, Hněvotínská 5, 779 00 Olomouc, Czech Republic
    • Petr Džubák
      Petr Džubák
      Institute of Molecular and Translational Medicine, Faculty of Medicine and Dentistry, Palacký University, Hněvotínská 5, 779 00 Olomouc, Czech Republic
    • Jan Hlaváč*
      Jan Hlaváč
      Department of Organic Chemistry, Faculty of Science, Palacký University, Tr. 17. Listopadu 12, 771 46 Olomouc, Czech Republic
      *Email: [email protected]
      More by Jan Hlaváč
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    Molecular Pharmaceutics

    Cite this: Mol. Pharmaceutics 2021, 18, 6, 2385–2396
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    https://doi.org/10.1021/acs.molpharmaceut.1c00219
    Published May 7, 2021
    Copyright © 2021 American Chemical Society

    Abstract

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    In this work, we report two concepts of drug delivery based on small-molecule drug conjugates with the ability of specific targeting and drug release monitoring via ratiometric fluorescence. The functionality of these concepts has been verified by two model systems consisting of three parts: (i) fluorescent aminoBODIPY for real-time detection of conjugate cleavage, (ii) a c(RGDfK) peptide specific for αvβ3 integrin receptors targeting angiogenesis in most solid tumors or redBODIPY for conjugate cleavage monitoring via FRET, and (iii) pegylated-2-phenyl-3-hydroxy-4(1H)-quinolinone (3HQ) as a model drug. The model drug release is based on a self-immolative disulfide linker sensitive to environments containing thiols, especially glutathione, which is overexpressed in cancer cells. The results show effective thiol-mediated cleavage of the fluorescent reporter and the subsequent liberation of the drug in a tube. The conjugate with c(RGDfK) was confirmed to penetrate the cells via interaction with integrin receptors. Drug release from this conjugate is possible to monitor inside the cells. Further, the synthetic approach to the conjugates and the method of fluorescence monitoring of the drug release have also been described.

    Copyright © 2021 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acs.molpharmaceut.1c00219.

    • NMR spectra of newly synthesized compounds; synthesis of the compounds 13 and 14 (PDF)

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    Cited By

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    This article is cited by 4 publications.

    1. Martin Porubský, Jiří Hodoň, Jarmila Stanková, Petr Džubák, Marián Hajdúch, Milan Urban, Jan Hlaváč. Near-infrared pH-switchable BODIPY photosensitizers for dual biotin/cRGD targeted photodynamic therapy. Journal of Photochemistry and Photobiology B: Biology 2024, 259 , 113010. https://doi.org/10.1016/j.jphotobiol.2024.113010
    2. Martin Porubsky, Jiří Hodoň, Jarmila Stanková, Petr Dzubak, Marian Hajduch, Milan Urban, Jan Hlaváč. Near-Infrared Ph-Switchable Bodipy Photosensitizers for Dual Biotin/Crgd Targeted Photodynamic Therapy. 2024https://doi.org/10.2139/ssrn.4854259
    3. Bhaskar C. Das, Parthiban Chokkalingam, Pavithra Masilamani, Srushti Shukla, Sasmita Das. Stimuli-Responsive Boron-Based Materials in Drug Delivery. International Journal of Molecular Sciences 2023, 24 (3) , 2757. https://doi.org/10.3390/ijms24032757
    4. Xu Zhang, Yanfei Zhu, Lihong Fan, Junhong Ling, Li-Ye Yang, Nan Wang, Xiao-kun Ouyang. Delivery of curcumin by fucoidan-coated mesoporous silica nanoparticles: Fabrication, characterization, and in vitro release performance. International Journal of Biological Macromolecules 2022, 211 , 368-379. https://doi.org/10.1016/j.ijbiomac.2022.05.086
    5. Zhou Xu, Qing-Xia Li, Lin-Wei Zhang, Mao-Long Chen, Jia Tu, Wei Chen, Ying-Yue Zhu, Yun-Hui Cheng. Target-modulated UCNPs-AChE assembly equipped with microenvironment-responsive immunosensor. Sensors and Actuators B: Chemical 2022, 352 , 131050. https://doi.org/10.1016/j.snb.2021.131050

    Molecular Pharmaceutics

    Cite this: Mol. Pharmaceutics 2021, 18, 6, 2385–2396
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.molpharmaceut.1c00219
    Published May 7, 2021
    Copyright © 2021 American Chemical Society

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