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Controlled Folding of Single Crystal Graphene
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    Controlled Folding of Single Crystal Graphene
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    Center for Multidimensional Carbon Materials (CMCM), Institute for Basic Science (IBS), Ulsan 44919, Republic of Korea
    SKKU Advanced Institute of Nano-Technology (SAINT), Department of Nano Science and Technology, Sungkyunkwan University, 2066 Seobu-ro, Jangan-gu, Suwon, Gyeonggi-do 16419, Republic of Korea
    § Department of Chemistry, Ulsan National Institute of Science and Technology (UNIST), Ulsan 44919, Republic of Korea
    School of Materials Science and Engineering, Ulsan National Institute of Science and Technology (UNIST), Ulsan 44919, Republic of Korea
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    Nano Letters

    Cite this: Nano Lett. 2017, 17, 3, 1467–1473
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    https://doi.org/10.1021/acs.nanolett.6b04459
    Published February 20, 2017
    Copyright © 2017 American Chemical Society

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    Folded graphene in which two layers are stacked with a twist angle between them has been predicted to exhibit unique electronic, thermal, and magnetic properties. We report the folding of a single crystal monolayer graphene film grown on a Cu(111) substrate by using a tailored substrate having a hydrophobic region and a hydrophilic region. Controlled film delamination from the hydrophilic region was used to prepare macroscopic folded graphene with good uniformity on the millimeter scale. This process was used to create many folded sheets each with a defined twist angle between the two sheets. By identifying the original lattice orientation of the monolayer graphene on Cu foil, or establishing the relation between the fold angle and twist angle, this folding technique allows for the preparation of twisted bilayer graphene films with defined stacking orientations and may also be extended to create folded structures of other two-dimensional nanomaterials.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.nanolett.6b04459.

    • Methods, SEM and TEM measurements of the single crystal monolayer graphene film, contact angle measurement of the modified substrate used for folding, photographs of the steps in the folding process, XPS spectrum of the FG, AFM measurement of the monolayer graphene, SEM image of the FG, alignment between graphene/Cu foil and the substrate for controlled folding, SAED patterns of FG-0°, FG-15°, and FG-30°, stacking model of two graphene monolayers with gradually changing rotational angles, Raman spectra of FG fabricated from polycrystalline monolayer graphene, electrical characterization of FG-based GFETs, the relation between the fold angle and the measured twist angle of FG samples, and statistics of carrier mobility from the GFET devices (PDF)

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    Nano Letters

    Cite this: Nano Lett. 2017, 17, 3, 1467–1473
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.nanolett.6b04459
    Published February 20, 2017
    Copyright © 2017 American Chemical Society

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