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Molecular n-Doping of Large- and Small-Diameter Carbon Nanotube Field-Effect Transistors with Tetrakis(tetramethylguanidino)benzene
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    Molecular n-Doping of Large- and Small-Diameter Carbon Nanotube Field-Effect Transistors with Tetrakis(tetramethylguanidino)benzene
    Click to copy article linkArticle link copied!

    • Jan M. Gotthardt
      Jan M. Gotthardt
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Severin Schneider
      Severin Schneider
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Maximilian Brohmann
      Maximilian Brohmann
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Simone Leingang
      Simone Leingang
      Institute for Inorganic Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Eric Sauter
      Eric Sauter
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
      More by Eric Sauter
    • Michael Zharnikov
      Michael Zharnikov
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Hans-Jörg Himmel
      Hans-Jörg Himmel
      Institute for Inorganic Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
    • Jana Zaumseil*
      Jana Zaumseil
      Institute for Physical Chemistry, Universität Heidelberg, D-69120 Heidelberg, Germany
      Centre for Advanced Materials, Universität Heidelberg, D-69120 Heidelberg, Germany
      *Email: [email protected]
    Other Access OptionsSupporting Information (1)

    ACS Applied Electronic Materials

    Cite this: ACS Appl. Electron. Mater. 2021, 3, 2, 804–812
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    https://doi.org/10.1021/acsaelm.0c00957
    Published January 26, 2021
    Copyright © 2021 The Authors. Published by American Chemical Society

    Abstract

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    The guanidino-functionalized aromatic compound 1,2,4,5-tetrakis(tetramethylguanidino)benzene (ttmgb) has been shown to be an efficient n-dopant for field-effect transistors (FETs) with gold contacts and networks of semiconducting single-walled carbon nanotubes (SWCNTs) with small diameters and large band gaps. Here, we investigate the broader applicability of ttmgb as a molecular n-dopant by fabricating bottom-contact/top-gate FETs with different air-stable, high work function metals as electrodes and with both small- and large-diameter polymer-sorted SWCNTs. Kelvin probe measurements indicate a reduction of the work functions of gold, palladium, and platinum by about 1 eV after ttmgb treatment and, correspondingly, gated four-point probe measurements show orders of magnitude lower contact resistances for electron injection into SWCNT networks. FETs based on networks of (6,5) SWCNTs with large band gaps as well as mixed semiconducting plasma torch SWCNTs with small band gaps can thus be transformed from ambipolar to purely n-type with no hole injection or increased off-currents by applying optimized ttmgb concentrations. Carrier concentration- and temperature-dependent measurements reveal that ttmgb treatment does not impact the electron transport and maximum mobilities in SWCNT networks at high carrier densities, but greatly improves the subthreshold slope of nanotube FETs by removing shallow electron trap states. This effect is found to be particularly pronounced for small-diameter nanotubes with large band gaps.

    Copyright © 2021 The Authors. Published by American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsaelm.0c00957.

    • Raman spectra of SWCNT dispersions; atomic force micrographs of SWCNT networks; transfer characteristics of (6,5) SWCNT FETs with different electrode materials; output characteristics of (6,5) SWCNT FETs with different electrode materials; transfer characteristics of plasma torch SWCNT FETs for different ttmgb concentrations; output characteristics of (6,5) and plasma torch SWCNT FETs with and without ttmgb treatment; and temperature-dependent onset voltages (PDF)

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    Most electronic Supporting Information files are available without a subscription to ACS Web Editions. Such files may be downloaded by article for research use (if there is a public use license linked to the relevant article, that license may permit other uses). Permission may be obtained from ACS for other uses through requests via the RightsLink permission system: http://pubs.acs.org/page/copyright/permissions.html.

    Cited By

    Click to copy section linkSection link copied!

    This article is cited by 11 publications.

    1. Sonja Wieland, Abdurrahman Ali El Yumin, Jan M. Gotthardt, Jana Zaumseil. Impact of Dielectric Environment on Trion Emission from Single-Walled Carbon Nanotube Networks. The Journal of Physical Chemistry C 2023, 127 (6) , 3112-3122. https://doi.org/10.1021/acs.jpcc.2c08338
    2. Nicolas F. Zorn, Felix J. Berger, Jana Zaumseil. Charge Transport in and Electroluminescence from sp3-Functionalized Carbon Nanotube Networks. ACS Nano 2021, 15 (6) , 10451-10463. https://doi.org/10.1021/acsnano.1c02878
    3. Daniil A. Ilatovskii, Dmitry V. Krasnikov, Daria S. Kopylova, Ayvaz I. Davletkhanov, Yuriy G. Gladush, Vladislav A. Kondrashov, Boris I. Afinogenov, Fedor M. Maksimov, Aleksandr Barulin, Vladislav V. Burdin, Alexander I. Chernov, Albert G. Nasibulin. Photophoretic deposition and separation of aerosol-synthesized single-walled carbon nanotubes. Carbon 2024, 218 , 118725. https://doi.org/10.1016/j.carbon.2023.118725
    4. Youngmin Han, Seongjae Kim, Chang-Hyun Kim, Hocheon Yoo. Experimental and Theoretical Evidence of Charge Injection Barrier Control by Small-Molecular Charge Injection Layer and Its Effects on Organic–Inorganic Complementary Inverters. IEEE Transactions on Electron Devices 2023, 70 (4) , 1710-1714. https://doi.org/10.1109/TED.2023.3247682
    5. Dongseong Yang, Kyoungtae Hwang, Yeon-Ju Kim, Yunseul Kim, Yina Moon, Nara Han, Minwoo Lee, Seung-Hoon Lee, Dong-Yu Kim. High-performance carbon nanotube field-effect transistors with electron mobility of 39.4 cm2V−1s−1 using anion–π interaction doping. Carbon 2023, 203 , 761-769. https://doi.org/10.1016/j.carbon.2022.12.025
    6. Wan Nor Roslam Wan Isahak, Lina Mohammed Shaker, Ahmed Al-Amiery. Oxygenated Hydrocarbons from Catalytic Hydrogenation of Carbon Dioxide. Catalysts 2023, 13 (1) , 115. https://doi.org/10.3390/catal13010115
    7. Shailesh S. Birajdar, Brendan Mirka, Vilas K. Gawade, Avinash L. Puyad, Benoît H. Lessard, Sidhanath V. Bhosale, Sheshanath V. Bhosale. Furan functionalized naphthalenediimide semiconductors with different N-alkyl chains for n-type organic thin-film transistor applications. Dyes and Pigments 2022, 206 , 110603. https://doi.org/10.1016/j.dyepig.2022.110603
    8. Anibal Pacheco-Sanchez, Quim Torrent, David Jiménez. Schottky-like barrier characterization of field-effect transistors with multiple quasi-ballistic channels. Journal of Applied Physics 2022, 132 (2) https://doi.org/10.1063/5.0091077
    9. Nicolas F. Zorn, Jana Zaumseil. Charge transport in semiconducting carbon nanotube networks. Applied Physics Reviews 2021, 8 (4) https://doi.org/10.1063/5.0065730
    10. Yuan Fang, Yang Zhang, Yuning Li, Jingye Sun, Mingqiang Zhu, Tao Deng. A novel temperature sensor based on three-dimensional buried-gate graphene field effect transistor. Nanotechnology 2021, 32 (48) , 485505. https://doi.org/10.1088/1361-6528/ac1f53
    11. Severin Schneider, Jan M. Gotthardt, Lena Steuer, Simone Leingang, Hans-Jörg Himmel, Jana Zaumseil. Improving electron injection and transport in polymer field-effect transistors with guanidino-functionalized aromatic n-dopants. Journal of Materials Chemistry C 2021, 9 (23) , 7485-7493. https://doi.org/10.1039/D1TC00968K

    ACS Applied Electronic Materials

    Cite this: ACS Appl. Electron. Mater. 2021, 3, 2, 804–812
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsaelm.0c00957
    Published January 26, 2021
    Copyright © 2021 The Authors. Published by American Chemical Society

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