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Converting Heat to Electrical Energy Using Highly Charged Polyoxometalate Electrolytes
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    Converting Heat to Electrical Energy Using Highly Charged Polyoxometalate Electrolytes
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    • Erik Svensson Grape
      Erik Svensson Grape
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
    • Jiawei Huang
      Jiawei Huang
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
      Oregon Center for Electrochemistry, University of Oregon, Eugene, Oregon 97403, United States
      More by Jiawei Huang
    • Dwaipayan Roychowdhury
      Dwaipayan Roychowdhury
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
      Oregon Center for Electrochemistry, University of Oregon, Eugene, Oregon 97403, United States
    • Tekalign T. Debela
      Tekalign T. Debela
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
    • Haeun Chang
      Haeun Chang
      Department of Chemistry and Biochemistry, University of California, San Diego, California 92093, United States
      More by Haeun Chang
    • Andrew Jenkins
      Andrew Jenkins
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
    • Alina M. Schimpf
      Alina M. Schimpf
      Department of Chemistry and Biochemistry, University of California, San Diego, California 92093, United States
      Program in Materials Science and Engineering, University of California, San Diego, California 92093, United States
    • Christopher H. Hendon
      Christopher H. Hendon
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
      Oregon Center for Electrochemistry, University of Oregon, Eugene, Oregon 97403, United States
    • Carl K. Brozek*
      Carl K. Brozek
      Department of Chemistry and Biochemistry, Material Science Institute, University of Oregon, Eugene, Oregon 97403, United States
      Oregon Center for Electrochemistry, University of Oregon, Eugene, Oregon 97403, United States
      *Email: [email protected]
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    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2024, 7, 24, 11423–11428
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    https://doi.org/10.1021/acsaem.4c00036
    Published March 27, 2024
    Copyright © 2024 American Chemical Society

    Abstract

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    Thermally regenerative electrochemical cycles and thermogalvanic cells harness redox entropy changes (ΔSrc) to interconvert heat and electricity with applications in heat harvesting and energy storage. Their efficiencies depend on ΔSrc because it relates directly to the Seebeck coefficient, yet few approaches exist for controlling the reaction entropy. Here, we demonstrate the design principle of using highly charged molecular species as electrolytes in thermogalvanic devices. As a proof-of-concept, the highly charged Wells-Dawson ion [P2W18O62]6– exhibits a large ΔSrc (−195 J mol–1 K–1) and a Seebeck coefficient comparable to state-of-the-art electrolytes (−1.7 mV K–1), demonstrating the potential of linking the rich chemistry of polyoxometalates to thermogalvanic technologies.

    Copyright © 2024 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsaem.4c00036.

    • All experimental details, spectroscopic data (IR, 31P NMR), cyclic voltammetry data, and thermogalvanic flow cell data (PDF)

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    Cited By

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    This article is cited by 2 publications.

    1. Mamta Dagar, Anyesh De, Zhou Lu, Ellen M. Matson, Agnes E. Thorarinsdottir. Implications of Charge and Heteroatom Dopants on the Thermodynamics and Kinetics of Redox Reactions in Keggin-Type Polyoxometalates. ACS Materials Au 2025, 5 (1) , 200-210. https://doi.org/10.1021/acsmaterialsau.4c00136
    2. Ashley N. Mapile, Erik Svensson Grape, Carl K. Brozek. Solvation of Nanoscale Materials. Chemistry of Materials 2024, 36 (19) , 9075-9088. https://doi.org/10.1021/acs.chemmater.4c01518

    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2024, 7, 24, 11423–11428
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsaem.4c00036
    Published March 27, 2024
    Copyright © 2024 American Chemical Society

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