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Direct Vapor Deposition Growth of 1T′ MoTe2 on Carbon Cloth for Electrocatalytic Hydrogen Evolution

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    Direct Vapor Deposition Growth of 1T′ MoTe2 on Carbon Cloth for Electrocatalytic Hydrogen Evolution
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    • Donglin Lu
      Donglin Lu
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Donglin Lu
    • Xiaohui Ren
      Xiaohui Ren
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Xiaohui Ren
    • Long Ren
      Long Ren
      Institute for Superconducting and Electronic Materials, Australian Institute for Innovative Materials, University of Wollongong, Innovation Campus, North Wollongong, New South Wales 2500, Australia
      More by Long Ren
    • Wenming Xue
      Wenming Xue
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Wenming Xue
    • Shenqian Liu
      Shenqian Liu
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Shenqian Liu
    • Yundan Liu
      Yundan Liu
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Yundan Liu
    • Qiong Chen
      Qiong Chen
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      More by Qiong Chen
    • Xiang Qi*
      Xiang Qi
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      *E-mail: [email protected]. (X.Q.).
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      Orcidhttp://orcid.org/0000-0002-0155-2558
    • Jianxin Zhong*
      Jianxin Zhong
      Hunan Key Laboratory for Micro-Nano Energy Materials and Devices, Laboratory for Quantum Engineering and Micro-Nano Energy Technology, and School of Physics and Optoelectronics, Xiangtan University, Xiangtan, Hunan 411105, People’s Republic of China
      *E-mail: [email protected] (J.Z.).
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    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2020, 3, 4, 3212–3219
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    https://doi.org/10.1021/acsaem.9b01589
    Published November 18, 2019
    Copyright © 2019 American Chemical Society
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    Abstract

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    Phase engineering has a profound effect on the chemical bonding and electric configuration, which play significant roles in regulating the activities of catalysts. The metallic phases of transition-metal dichalcogenides (TMDs) have been proposed to show more excellent performance in electrocatalysis over their semiconductor phase; however, the controllable phase engineering for these compounds remains a challenge. In this work, filmlike 1T′ MoTe2 (F-1T′ MoTe2), filmlike 1T′/2H MoTe2, porous 1T′ MoTe2, small granular 1T′ MoTe2, and large granular 1T′ MoTe2 were successfully synthesized on a flexible carbon cloth (CC) substrate with 3D network structure by chemical vapor deposition (CVD). The high activity of the as-synthesized F-1T′ MoTe2/CC electrode for HER in 1 M H2SO4 solution was demonstrated by the small onset overpotential of −230.7 mV, a low Tafel slope of 127.1 mV dec–1, and robust electrochemical durability. The enhanced electrocatalytic activity and stability of F-1T′ MoTe2/CC benefit from excellent catalytically active sites and remarkable conductivity of the F-1T′ MoTe2. The results demonstrate an efficient route to designing and constructing metallic-phase TMD catalysts for high-performance electrocatalytic devices.

    Copyright © 2019 American Chemical Society

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    Supporting Information

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    • Detailed experiment and calculation method; XRD patterns of MoO2/CC and MoO2/MoTe2/CC mixtures; SEM images of CC, as-prepared F-1T′/2H MoTe2/CC, P-1T′ MoTe2/CC, SG-1T′ MoTe2/CC, LG-1T′MoTe2/CC, and tested P-1T′ MoTe2/CC or LG-1T′MoTe2/CC; band structure of 2H MoTe2 and 1T′ MoTe2; hydrogen atom adsorption in different positions on MoTe2 and their corresponding values of ΔGH calculated by DFT simulation; CV behaviors of F-1T′ MoTe2/CC and F-1T′/2H MoTe2/CC; maximum current density at each sweep speed C[H+] for F-1T′ MoTe2/CC and F-1T′/2H MoTe2/CC; and SEM images and Raman spectra of the HER tested samples (PDF)

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    This article is cited by 54 publications.

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    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2020, 3, 4, 3212–3219
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsaem.9b01589
    Published November 18, 2019
    Copyright © 2019 American Chemical Society
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