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Exploring the Interfacial Chemistry between Zinc Anodes and Aqueous Electrolytes via an In Situ Visualized Characterization System

  • Xunzhu Zhou
    Xunzhu Zhou
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Xunzhu Zhou
  • Yong Lu
    Yong Lu
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Yong Lu
  • Qiu Zhang
    Qiu Zhang
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Qiu Zhang
  • Licheng Miao
    Licheng Miao
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Licheng Miao
  • Kai Zhang
    Kai Zhang
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Kai Zhang
  • Zhenhua Yan
    Zhenhua Yan
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    More by Zhenhua Yan
  • Fujun Li*
    Fujun Li
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    *Email: [email protected]
    More by Fujun Li
  • , and 
  • Jun Chen*
    Jun Chen
    Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Renewable Energy Conversion and Storage Centre (RECAST), College of Chemistry, Nankai University, Tianjin 300071, P. R. China
    *Email: [email protected]
    More by Jun Chen
Cite this: ACS Appl. Mater. Interfaces 2020, 12, 49, 55476–55482
Publication Date (Web):November 25, 2020
https://doi.org/10.1021/acsami.0c17023
Copyright © 2020 American Chemical Society

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    Abstract

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    Direct monitoring of dendrite growth, hydrogen evolution, and surface passivation can enrich the chemical and morphological understanding of the unstable Zn/electrolyte interface and provide guidelines for rational design of Zn anodes; however, the on-line observation with high precision is hitherto lacking. Herein, we present a real-time comprehensive characterization system, including in situ atomic force microscopy, optical microscopy, and electrochemical quartz crystal microbalance (referred to as the “3M” system), to provide multiscale views on the semisphere nuclei and growth of bump-like dendrites and the potential-dependent chemical and morphological structures of passivated products in a mild acidic electrolyte. It is revealed that the poor interfacial properties can be attributed to the sparse nucleation sites and direct contact of Zn with the electrolyte. The 3M system further visualizes and confirms that the additive polyethylene glycol acts as a Zn2+ distribution promoter and physical barrier and merits stable electrochemical performance.

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsami.0c17023.

    • Preparation process, photograph and 3D AFM height image of homemade planar electrode; XRD pattern; AFM height image; optical cross-sectional observations; enlarged AFM image; image captured by an optical camera; morphology and corresponding height; configurations and bonding energies; LSV curves; contact angles; physical properties; FTIR; electrochemical impedance spectroscopy; cycling curves of Coulombic efficiency; summary of recently reported strategies; comparison of electrochemical performance; and comparison of critical nucleation radius and areal nuclei density (PDF)

    • The visualized hydrogen evolution in 1 M ZnSO4 electrolyte (MP4)

    • The visualized hydrogen evolution in 1 M ZnSO4-1000 ppm PEG electrolyte (MP4)

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    This article is cited by 63 publications.

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