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NO Photoreleaser-Deoxyadenosine and -Bile Acid Derivative Bioconjugates as Novel Potential Photochemotherapeutics
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    NO Photoreleaser-Deoxyadenosine and -Bile Acid Derivative Bioconjugates as Novel Potential Photochemotherapeutics
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    ISOF-CNR, via P. Gobetti, 101, 40129 Bologna, Italy
    Laboratory of Photochemistry, Department of Drug Sciences, University of Catania, 95125 Catania, Italy
    § Department of Chemical and Pharmaceutical Sciences, University of Ferrara, via L. Borsari, 46, 44121 Ferrara, Italy
    Department of Medical Sciences, University of Ferrara, corso Giovecca, 203, 44121 Ferrara, Italy
    Department of Bio-Medical and Biotechnological Sciences, Physiology Division, University of Catania, I-95125 Catania, Italy
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    ACS Medicinal Chemistry Letters

    Cite this: ACS Med. Chem. Lett. 2016, 7, 10, 939–943
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    https://doi.org/10.1021/acsmedchemlett.6b00257
    Published August 18, 2016
    Copyright © 2016 American Chemical Society

    Abstract

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    This contribution reports the synthesis of some novel bioconjugates with anticancer activity and able to release nitric oxide (NO) under visible light excitation. The 4-nitro-2-(trifluoromethyl)aniline derivative, a suitable NO photodonor, was conjugated with 2′-deoxyadenosine and urso- and cheno-deoxycholic acid derivatives, through a thioalkylic chain or the 4-alkyl-1,2,3-triazole moiety. Photochemical experiments demonstrated the effective release of NO from 2′-deoxyadenosine and ursodeoxycholic acid conjugates under the exclusive control of visible light inputs. Studies for the in vitro antiproliferative activity against leukemic K562 and colon carcinoma HCT116 cell lines are reported for all the compounds as well as a case study of photocytotoxicity against HCT116.

    Copyright © 2016 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acsmedchemlett.6b00257.

    • General experimental information; full synthetic procedures and characterization data for all new compounds; experimental procedures for the biological assay (PDF)

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    Cited By

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    This article is cited by 14 publications.

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    2. Neha V. Rathod, Satyendra Mishra. Bile Acid-conjugate as a Promising Anticancer Agent: Recent Progress. Current Medicinal Chemistry 2024, 31 (26) , 4160-4179. https://doi.org/10.2174/0109298673274040231121113410
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    6. Maria Chiara di Gregorio, Jacopo Cautela, Luciano Galantini. Physiology and Physical Chemistry of Bile Acids. International Journal of Molecular Sciences 2021, 22 (4) , 1780. https://doi.org/10.3390/ijms22041780
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    9. Ronghua Shen, Ying Qian. A turn-on and lysosome-targeted fluorescent NO releaser in water media and its application in living cells and zebrafishes. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 2020, 230 , 118024. https://doi.org/10.1016/j.saa.2019.118024
    10. Nancy Sharma, Ajay Kumar Dhyani, Srujan Marepally, D. Amilan Jose. Nanoscale lipid vesicles functionalized with a nitro-aniline derivative for photoinduced nitric oxide (NO) delivery. Nanoscale Advances 2020, 2 (1) , 463-469. https://doi.org/10.1039/C9NA00532C
    11. Zhi Xu, Shi-Jia Zhao, Yi Liu. 1,2,3-Triazole-containing hybrids as potential anticancer agents: Current developments, action mechanisms and structure-activity relationships. European Journal of Medicinal Chemistry 2019, 183 , 111700. https://doi.org/10.1016/j.ejmech.2019.111700
    12. Jean-François Goossens, Christian Bailly. Ursodeoxycholic acid and cancer: From chemoprevention to chemotherapy. Pharmacology & Therapeutics 2019, 203 , 107396. https://doi.org/10.1016/j.pharmthera.2019.107396
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    14. Maria Navacchia, Elena Marchesi, Lara Mari, Nicola Chinaglia, Eleonora Gallerani, Riccardo Gavioli, Massimo Capobianco, Daniela Perrone. Rational Design of Nucleoside–Bile Acid Conjugates Incorporating a Triazole Moiety for Anticancer Evaluation and SAR Exploration. Molecules 2017, 22 (10) , 1710. https://doi.org/10.3390/molecules22101710

    ACS Medicinal Chemistry Letters

    Cite this: ACS Med. Chem. Lett. 2016, 7, 10, 939–943
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsmedchemlett.6b00257
    Published August 18, 2016
    Copyright © 2016 American Chemical Society

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