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Dynamic Manipulation in Piezoresponse Force Microscopy: Creating Nonequilibrium Phases with Large Electromechanical Response
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    Dynamic Manipulation in Piezoresponse Force Microscopy: Creating Nonequilibrium Phases with Large Electromechanical Response
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    • Kyle P. Kelley*
      Kyle P. Kelley
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
      *Email: [email protected]
    • Yao Ren
      Yao Ren
      Department of Materials Science and Engineering, University of Texas at Arlington, Arlington, Texas 76019, United States
      More by Yao Ren
    • Anna N. Morozovska
      Anna N. Morozovska
      Institute of Physics, National Academy of Science of Ukraine, Pr. Nauki 46, 03028 Kyiv, Ukraine
    • Eugene A. Eliseev
      Eugene A. Eliseev
      Institute for Problems of Materials Science, National Academy of Science of Ukraine, Krjijanovskogo 3, 03142 Kyiv, Ukraine
    • Yoshitaka Ehara
      Yoshitaka Ehara
      Department of Communications Engineering, National Defense Academy, Hashirimizu, Yokosuka, 239-8686, Japan
      Department of Material Science and Engineering, Tokyo Institute of Technology, Yokohama 226-8502, Japan
    • Hiroshi Funakubo
      Hiroshi Funakubo
      Department of Material Science and Engineering, Tokyo Institute of Technology, Yokohama 226-8502, Japan
    • Thierry Giamarchi
      Thierry Giamarchi
      Department of Quantum Matter Physics, University of Geneva, 24 Quai Ernest-Ansermet, CH-1211 Geneva, Switzerland
    • Nina Balke
      Nina Balke
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
      More by Nina Balke
    • Rama K. Vasudevan
      Rama K. Vasudevan
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
    • Ye Cao
      Ye Cao
      Department of Materials Science and Engineering, University of Texas at Arlington, Arlington, Texas 76019, United States
      More by Ye Cao
    • Stephen Jesse
      Stephen Jesse
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
    • Sergei V. Kalinin*
      Sergei V. Kalinin
      Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
      *Email: [email protected]
    Other Access OptionsSupporting Information (1)

    ACS Nano

    Cite this: ACS Nano 2020, 14, 8, 10569–10577
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    https://doi.org/10.1021/acsnano.0c04601
    Published August 6, 2020
    Copyright © 2020 American Chemical Society

    Abstract

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    Domain walls and topological defects in ferroelectric materials have emerged as a powerful tool for functional electronic devices including memory and logic. Similarly, wall interactions and dynamics underpin a broad range of mesoscale phenomena ranging from giant electromechanical responses to memory effects. Exploring the functionalities of individual domain walls, their interactions, and controlled modifications of the domain structures is crucial for applications and fundamental physical studies. However, the dynamic nature of these features severely limits studies of their local physics since application of local biases or pressures in piezoresponse force microscopy induce wall displacement as a primary response. Here, we introduce an approach for the control and modification of domain structures based on automated experimentation, whereby real-space image-based feedback is used to control the tip bias during ferroelectric switching, allowing for modification routes conditioned on domain states under the tip. This automated experiment approach is demonstrated for the exploration of domain wall dynamics and creation of metastable phases with large electromechanical response.

    Copyright © 2020 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsnano.0c04601.

    • Additional information including equation derivations, phase field modeling, and relevant experiments (PDF)

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    Cited By

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    This article is cited by 15 publications.

    1. Kyle P. Kelley, Yao Ren, Arvind Dasgupta, Pravin Kavle, Stephen Jesse, Rama K. Vasudevan, Ye Cao, Lane W. Martin, Sergei V. Kalinin. Probing Metastable Domain Dynamics via Automated Experimentation in Piezoresponse Force Microscopy. ACS Nano 2021, 15 (9) , 15096-15103. https://doi.org/10.1021/acsnano.1c05455
    2. Sergei V. Kalinin, Maxim Ziatdinov, Jacob Hinkle, Stephen Jesse, Ayana Ghosh, Kyle P. Kelley, Andrew R. Lupini, Bobby G. Sumpter, Rama K. Vasudevan. Automated and Autonomous Experiments in Electron and Scanning Probe Microscopy. ACS Nano 2021, 15 (8) , 12604-12627. https://doi.org/10.1021/acsnano.1c02104
    3. Rama K. Vasudevan, Kyle P. Kelley, Jacob Hinkle, Hiroshi Funakubo, Stephen Jesse, Sergei V. Kalinin, Maxim Ziatdinov. Autonomous Experiments in Scanning Probe Microscopy and Spectroscopy: Choosing Where to Explore Polarization Dynamics in Ferroelectrics. ACS Nano 2021, 15 (7) , 11253-11262. https://doi.org/10.1021/acsnano.0c10239
    4. Run-Lin Liu, Jian Wang, Zhong-Hui Shen, Yang Shen. AI for dielectric capacitors. Energy Storage Materials 2024, 71 , 103612. https://doi.org/10.1016/j.ensm.2024.103612
    5. Yongtao Liu, Rama K. Vasudevan, Kyle P. Kelley, Hiroshi Funakubo, Maxim Ziatdinov, Sergei V. Kalinin. Learning the right channel in multimodal imaging: automated experiment in piezoresponse force microscopy. npj Computational Materials 2023, 9 (1) https://doi.org/10.1038/s41524-023-00985-x
    6. Pravin Kavle, Aiden M. Ross, Jacob A. Zorn, Piush Behera, Eric Parsonnet, Xiaoxi Huang, Ching‐Che Lin, Lucas Caretta, Long‐Qing Chen, Lane W. Martin. Exchange‐Interaction‐Like Behavior in Ferroelectric Bilayers. Advanced Materials 2023, 35 (39) https://doi.org/10.1002/adma.202301934
    7. Mani Valleti, Rama K. Vasudevan, Maxim A. Ziatdinov, Sergei V. Kalinin. Bayesian optimization in continuous spaces via virtual process embeddings. Digital Discovery 2022, 1 (6) , 910-925. https://doi.org/10.1039/D2DD00065B
    8. Kevin M. Roccapriore, Sergei V. Kalinin, Maxim Ziatdinov. Physics Discovery in Nanoplasmonic Systems via Autonomous Experiments in Scanning Transmission Electron Microscopy. Advanced Science 2022, 9 (36) https://doi.org/10.1002/advs.202203422
    9. Shivaranjan Raghuraman, Yongtao Liu, Kyle Kelley, Rama K Vasudevan, Stephen Jesse. Python and FPGA-based Workflow for Automated and Interoperable Scanning Probe Microscopy. Microscopy and Microanalysis 2022, 28 (S1) , 3114-3115. https://doi.org/10.1017/S143192762201159X
    10. Wenping Geng, Xiaojun Qiao, Jinlong He, Huifen Wei, Dongwan Zheng, Gang Xue, Caiqin Zhao, Jianwei Meng, Kaixi Bi, Junbin Yu, Yikun Shi, Xiujian Chou. Domain reversal and current transport property in BiFeO3 films. Ceramics International 2022, 48 (13) , 18151-18156. https://doi.org/10.1016/j.ceramint.2022.03.073
    11. Yongtao Liu, Shelby S. Fields, Takanori Mimura, Kyle P. Kelley, Susan Trolier-McKinstry, Jon F. Ihlefeld, Sergei V. Kalinin. Exploring leakage in dielectric films via automated experiments in scanning probe microscopy. Applied Physics Letters 2022, 120 (18) https://doi.org/10.1063/5.0079217
    12. Yongtao Liu, Kyle P. Kelley, Rama K. Vasudevan, Hiroshi Funakubo, Maxim A. Ziatdinov, Sergei V. Kalinin. Experimental discovery of structure–property relationships in ferroelectric materials via active learning. Nature Machine Intelligence 2022, 4 (4) , 341-350. https://doi.org/10.1038/s42256-022-00460-0
    13. Wenping Geng, Xiaojun Qiao, Caiqin Zhao, Dongwan Zheng, Yaqing Li, Le Zhang, Kaixi Bi, Yun Yang, Yao Sun, Xiujian Chou. Temperature dependence of ferroelectric property and leakage mechanism in Mn-doped Pb(Zr0.3Ti0.7)O3 films. Ceramics International 2021, 47 (17) , 24047-24052. https://doi.org/10.1016/j.ceramint.2021.05.114
    14. Dongyu He, Xiujian Tang, Yuxin Liu, Jian Liu, Wenbo Du, Pengfei He, Haidou Wang. Phase Transition Effect on Ferroelectric Domain Surface Charge Dynamics in BaTiO3 Single Crystal. Materials 2021, 14 (16) , 4463. https://doi.org/10.3390/ma14164463
    15. Seungbum Hong. Single frequency vertical piezoresponse force microscopy. Journal of Applied Physics 2021, 129 (5) https://doi.org/10.1063/5.0038744

    ACS Nano

    Cite this: ACS Nano 2020, 14, 8, 10569–10577
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsnano.0c04601
    Published August 6, 2020
    Copyright © 2020 American Chemical Society

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