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Biomimetic Surface-Enhanced Raman Scattering Nanoparticles with Improved Dispersibility, Signal Brightness, and Tumor Targeting Functions
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    Biomimetic Surface-Enhanced Raman Scattering Nanoparticles with Improved Dispersibility, Signal Brightness, and Tumor Targeting Functions
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    • Indrajit Srivastava
      Indrajit Srivastava
      Department of Bioengineering  and  Department of Electrical and Computer Engineering, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
    • Ruiyang Xue
      Ruiyang Xue
      Department of Materials Science and Engineering, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
      More by Ruiyang Xue
    • Jamie Jones
      Jamie Jones
      Department of Bioengineering, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
      More by Jamie Jones
    • Hyunjoon Rhee
      Hyunjoon Rhee
      Department of Bioengineering, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
    • Kristen Flatt
      Kristen Flatt
      Materials Research Laboratories Central Research Facilities, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
    • Viktor Gruev*
      Viktor Gruev
      Department of Electrical and Computer Engineering  and  Carle Illinois College of Medicine, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
      *Email: [email protected]
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    • Shuming Nie*
      Shuming Nie
      Department of Bioengineering,  Department of Electrical and Computer Engineering,  Department of Materials Science and Engineering,  Department of Chemistry  and  Carle Illinois College of Medicine, University of Illinois at Urbana−Champaign, Urbana, Illinois 61801, United States
      *Email: [email protected]
      More by Shuming Nie
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    ACS Nano

    Cite this: ACS Nano 2022, 16, 5, 8051–8063
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    https://doi.org/10.1021/acsnano.2c01062
    Published April 26, 2022
    Copyright © 2022 American Chemical Society

    Abstract

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    The development of biocompatible and nontoxic surface-enhanced Raman scattering (SERS) nanoparticles is of considerable current interest because of their attractive biomedical applications such as ultrasensitive in vitro diagnostics, in vivo tumor imaging, and spectroscopy-guided cancer surgery. However, current SERS nanoparticles are prepared and stored in aqueous solution, have limited stability and dispersibility, and are not suitable for lyophilization and storage by freeze-drying or other means. Here, we report a simple but robust method to coat colloidal SERS nanoparticles by naturally derived biomimetic red blood cell membranes (RBCM), leading to a dramatic improvement in stability and dispersibility under freeze–thawing, lyophilization, heating, and physiological conditions. The results demonstrate that the lyophilized SERS nanoparticles in the solid form can be readily dissolved and dispersed in physiological buffer solutions. A surprising finding is that the RBCM-coated SERS particles are considerably brighter (by as much as 5-fold) than PEGylated SERS particles under similar experimental conditions. This additional enhancement is believed to arise from the hydrophobic nature of RBCM’s hydrocarbon chains, which is known to reduce electronic dampening and boost electromagnetic field enhancement. A further advantage in using biomimetic membrane coatings is that the bilayer membrane structure allows nonvalent insertion of molecular ligands for tumor targeting. In particular, we show that cyclic-RGD, a tumor-targeting peptide, can be efficiently inserted into the membrane coatings of SERS nanoparticles for targeting the ανβ3 integrin receptors expressed on cancer cells. Thus, biomimetic RBCMs provide major advantages over traditional polyethylene glycols for preparing SERS nanoparticles with improved dispersibility, higher signal intensity, and more efficient biofunctionalization.

    Copyright © 2022 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsnano.2c01062.

    • Further details on enhancement factor calculations, and 25 figures of experimental data showing: (1) UV–vis absorption spectra of PEGylated AuNPs, (2) improved dispersion stability of various size and anisotropic AuNPs, (3) negative-stained TEM, (4) physiological stability data of AuNP-RBCMs, (5) SERS signal stability data of AuNPs upon freeze–thaw and lyophilization cycles, (6) lipid-insertion optimization data, (7) cellular toxicity data of AuNP-RBCMs, and (8) in vitro SERS spectra of AuNP-RBCMs in PANC-1 cells (PDF)

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    Cited By

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    This article is cited by 18 publications.

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    ACS Nano

    Cite this: ACS Nano 2022, 16, 5, 8051–8063
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsnano.2c01062
    Published April 26, 2022
    Copyright © 2022 American Chemical Society

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