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Simple Synthesis of Nanocrystalline Tin Sulfide/N-Doped Reduced Graphene Oxide Composites as Lithium Ion Battery Anodes

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    Simple Synthesis of Nanocrystalline Tin Sulfide/N-Doped Reduced Graphene Oxide Composites as Lithium Ion Battery Anodes
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    † Department of Chemical Engineering and Department of Chemistry, Center for Electrochemistry, University of Texas at Austin, 1 University Station, C0400 Austin, Texas 78712-0231, United States
    ‡ Department of Chemistry and the Institute for Computational Engineering and Sciences, University of Texas at Austin, Austin, Texas 78712-0165, United States
    § Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang, 790-784, South Korea
    ∥ Texas Materials Institute, University of Texas at Austin, Austin, Texas 78712-1591, United States
    *E-mail: [email protected]
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    ACS Nano

    Cite this: ACS Nano 2016, 10, 12, 10778–10788
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    https://doi.org/10.1021/acsnano.6b04214
    Published November 22, 2016
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    Composites of nitrogen-doped reduced graphene oxide (NRGO) and nanocrystalline tin sulfides were synthesized, and their performance as lithium ion battery anodes was evaluated. Following the first cycle the composite consisted of Li2S/LixSn/NRGO. The conductive NRGO cushions the stress associated with the expansion of lithiation of Sn, and the noncycling Li2S increases the residual Coulombic capacity of the cycled anode because (a) Sn domains in the composite formed of unsupported SnS2 expand only by 63% while those in the composite formed of unsupported SnS expand by 91% and (b) Li percolates rapidly at the boundary between the Li2S and LixSn nanodomains. The best cycling SnS2/NRGO-derived composite retained a specific capacity of 562 mAh g–1 at the 200th cycle at 0.2 A g–1 rate.

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