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Hierarchical 3D Architectured Ag Nanowires Shelled with NiMn-Layered Double Hydroxide as an Efficient Bifunctional Oxygen Electrocatalyst

  • Soressa Abera Chala
    Soressa Abera Chala
    NanoElectrochemistry Laboratory, Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    Sustainable Energy Development Center, National Taiwan University of Science and Technology, Taipei 106, Taiwan
  • Meng-Che Tsai*
    Meng-Che Tsai
    NanoElectrochemistry Laboratory, Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    Sustainable Energy Development Center, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    *E-mail: [email protected]
  • Wei-Nien Su*
    Wei-Nien Su
    NanoElectrochemistry Laboratory, Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    Sustainable Energy Development Center, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    *E-mail: [email protected]
    More by Wei-Nien Su
  • Kassa Belay Ibrahim
    Kassa Belay Ibrahim
    NanoElectrochemistry Laboratory, Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 106, Taiwan
  • Balamurugan Thirumalraj
    Balamurugan Thirumalraj
    NanoElectrochemistry Laboratory, Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    Sustainable Energy Development Center, National Taiwan University of Science and Technology, Taipei 106, Taiwan
  • Ting-Shan Chan
    Ting-Shan Chan
    National Synchrotron Radiation Research Center, Hsin-Chu 30076, Taiwan
  • Jyh-Fu Lee
    Jyh-Fu Lee
    National Synchrotron Radiation Research Center, Hsin-Chu 30076, Taiwan
    More by Jyh-Fu Lee
  • Hongjie Dai*
    Hongjie Dai
    Department of Chemistry, Stanford University, Stanford, California 94305, United States
    *E-mail: [email protected]
    More by Hongjie Dai
  • , and 
  • Bing-Joe Hwang*
    Bing-Joe Hwang
    NanoElectrochemistry Laboratory, Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    NanoElectrochemistry Laboratory, Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    Sustainable Energy Development Center, National Taiwan University of Science and Technology, Taipei 106, Taiwan
    National Synchrotron Radiation Research Center, Hsin-Chu 30076, Taiwan
    *E-mail: [email protected]
Cite this: ACS Nano 2020, 14, 2, 1770–1782
Publication Date (Web):January 31, 2020
https://doi.org/10.1021/acsnano.9b07487
Copyright © 2020 American Chemical Society

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    Abstract

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    Herein, we report hierarchical 3D NiMn-layered double hydroxide (NiMn-LDHs) shells grown on conductive silver nanowire (Ag NWs) cores as efficient, low-cost, and durable oxygen reduction reaction (ORR)/oxygen evolution reaction (OER) bifunctional electrocatalysts for metal–air batteries. The hierarchical 3D architectured Ag NW@NiMn-LDH catalysts exhibit superb OER/ORR activities in alkaline conditions. The outstanding bifunctional activities of Ag NW@NiMn-LDHs are essentially attributed to increasing both site activity and site populations. The synergistic contributions from the hierarchical 3D open-pore structure of the LDH shells, improved electrical conductivity, and small thickness of the LDHs shells are associated with more accessible site populations. Moreover, the charge transfer between Ag cores and metals of LDH shells and the formation of defective and distorted sites (less coordinated Ni and Mn sites) strongly enhance the site activity. Thus, Ag NW@NiMn-LDH hybrids exhibit a 0.75 V overvoltage difference between ORR and OER with excellent durability for 30 h, demonstrating the distinguished bifunctional electrocatalyst reported to date. Interestingly, the homemade rechargeable Zn–air battery using the hybrid Ag NW@NiMn-LDHs (1:2) catalyst as the air electrode exhibits a charge–discharge voltage gap of ∼0.77 V at 10 mA cm–2 and shows excellent cycling stability. Thus, the concept of the hierarchical 3D architecture of Ag NW@NiMn-LDHs considerably advances the practice of LDHs toward metal–air batteries and oxygen electrocatalysts.

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsnano.9b07487.

    • Additional SEM images, TEM (before and after long-time stability test), HR-TEM (before and after long-time stability test), EDX, XRD, FT-IR, BET, Raman spectra, XPS (before and after long-time stability test), XANES and EXAFS analysis, electrochemical results (CV, LSV, ECSA, and durability), conductivity result measured by 4-pont probe, EIS, computational DFT calculations, and performance comparison table (PDF)

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