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Crystal Structure and Magnetic Properties of a New Two-Dimensional S = 1 Quantum Spin System Ni5(TeO3)4X2 (X = Cl, Br)

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    Crystal Structure and Magnetic Properties of a New Two-Dimensional S = 1 Quantum Spin System Ni5(TeO3)4X2 (X = Cl, Br)
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    Department of Inorganic Chemistry, Stockholm University, S-106 91 Stockholm, Sweden, Department of Chemistry, University of Bergen, Allégt. 41, 5007 Bergen, Norway, Max Planck Institute for Solid State Research, Heisenbergstrasse 1, D-70569 Stuttgart, Germany, and Centre d'Elaboration de Matériaux et d'Etudes Structurales (CEMES/CNRS), 29 rue Jeanne Marvig, BP 4347, Toulouse Cedex 4, France
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    Cite this: Chem. Mater. 2003, 15, 1, 68–73
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    https://doi.org/10.1021/cm0206587
    Published November 12, 2002
    Copyright © 2003 American Chemical Society
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    Two new transition-metal tellurium oxy-chlorides of the general formula Ni5(TeO3)4X2 (X = Cl, Br) have been isolated during the investigation of the ternary phase diagram NiO−NiCl2−TeO2. They crystallize in the monoclinic system, space group C2/c, and for the case of Ni5(TeO3)4Cl2 the unit cell is a = 19.5674(2) Å, b = 5.2457(1) Å, and c = 16.3084(1) Å, with β = 125.289(1)°. The structure is layered and built up of corner-connected [Ni5O17X2] entities, made of five nickel(II) octahedra associated by edge and face sharing. The tellurium(IV) atoms are fixed upon the nickel layers. Their lone pairs E and the halogen atoms are packed in a double layer perpendicular to the [010] direction. From the magnetic point of view, this system provides a new 2D S = 1 quantum spin system with antiferromagnetic superexchange interaction. The magnetic susceptibility shows anomalies pointing to magnetic ordering phenomena. The observed transition temperatures vary with the interlayer separation.

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    †

     Stockholm University.

    ‡

     University of Bergen.

    §

     Max Planck Institute for Solid State Research.

    *

     To whom correspondence should be addressed. Tel.:  33 5 62 25 78 28. Fax:  33 5 62 25 79 99. E-mail:  [email protected].

    ‖

     Centre d'Elaboration de Matériaux et d'Etudes Structurales (CEMES/CNRS).

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    Cite this: Chem. Mater. 2003, 15, 1, 68–73
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    https://doi.org/10.1021/cm0206587
    Published November 12, 2002
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