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Large-Scale Separation of Metallic and Semiconducting Single-Walled Carbon Nanotubes

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Contribution from the Department of Chemistry, Tokyo Gakugei University, Tokyo 184-8501, Japan, Center for Tsukuba Advanced Research Alliance, University of Tsukuba, Tsukuba 305-8577, Japan, Mesoscopic Physics Laboratory, Department of Physics, Peking University, Beijing 100871, People's Republic of China, Department of Theoretical Molecular Science, Institute for Molecular Science, Okazaki 444-8585, Japan, National Laboratory of Advanced Industrial Science and Technology, Tsukuba 305-8565, Japan, Research Institute for Electronic Science, Hokkaido University, Sapporo 060-0812, Japan, Department of Chemistry, Graduate School of Science, Tohoku University, Sendai 980-8578, Japan
Cite this: J. Am. Chem. Soc. 2005, 127, 29, 10287–10290
Publication Date (Web):July 1, 2005
https://doi.org/10.1021/ja051774o
Copyright © 2005 American Chemical Society
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Abstract

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In the applications of single-walled carbon nanotubes (SWNTs), it is extremely important to separate semiconducting and metallic SWNTs. Although several methods have been reported for the separation, only low yields have been achieved at great expense. We show a separation method involving a dispersion−centrifugation process in a tetrahydrofuran solution of amine, which makes metallic SWNTs highly concentrated to 87% in a simple way.

†

 Tokyo Gakugei University.

‡

 University of Tsukuba.

*

In papers with more than one author, the asterisk indicates the name of the author to whom inquiries about the paper should be addressed.

§

 Peking University.

‖

 Institute for Molecular Science.

⊥

 AIST.

#

 Hokkaido University.

○

 Tohoku University.

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SEM images of AP-SWNTs and SWNTs-OS1. AFM image and cross-sectional profile of SWNTs-OS1. This material is available free of charge via the Internet at http://pubs.acs.org.

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