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    Predominant (6,5) Single-Walled Carbon Nanotube Growth on a Copper-Promoted Iron Catalyst
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    Department of Biotechnology and Chemical Technology, School of Science and Technology, Aalto University, P.O. Box 16100, FI-00076 Aalto, Finland, A. M. Prokhorov General Physics Institute, Russian Academy of Sciences, 38 Vavilov Street, 119991 Moscow, Russia, Department of Applied Physics, School of Science and Technology, Aalto University, P.O. Box 11100, FI-00076 Aalto, Finland, NanoMaterials Group, Department of Applied Physics, and Center for New Materials, School of Science and Technology, Aalto University, P.O. Box 15100, FI-00076 Aalto, Finland, and VTT Biotechnology, P.O. Box 1000, FI-02044, Espoo, Finland
    [email protected]; [email protected]
    †Department of Biotechnology and Chemical Technology, Aalto University.
    ‡A. M. Prokhorov General Physics Institute.
    §Department of Applied Physics, Aalto University.
    ∥NanoMaterials Group, Department of Applied Physics, and Center for New Materials, Aalto University.
    ⊥VTT Biotechnology.
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    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2010, 132, 40, 13994–13996
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    https://doi.org/10.1021/ja106609y
    Published September 21, 2010
    Copyright © 2010 American Chemical Society
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    Abstract

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    We have developed a magnesia (MgO)-supported iron−copper (FeCu) catalyst to accomplish the growth of single-walled carbon nanotubes (SWNTs) using carbon monoxide (CO) as the carbon source at ambient pressure. The FeCu catalyst system facilitates the growth of small-diameter SWNTs with a narrow diameter distribution. UV−vis−NIR optical absorption spectra and photoluminescence excitation (PLE) mapping were used to evaluate the relative quantities of the different (n,m) species. We have also demonstrated that the addition of Cu to the Fe catalyst can also cause a remarkable increase in the yield of SWNTs. Finally, a growth mechanism for the FeCu-catalyzed synthesis of SWNTs has been proposed.

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    Experimental details of the catalyst preparation and the carbon nanotube growth as well as characterizations. This material is available free of charge via the Internet at http://pubs.acs.org.

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    Cite this: J. Am. Chem. Soc. 2010, 132, 40, 13994–13996
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