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Vapochromic Behavior of a Chair-Shaped Supramolecular Metallacycle with Ultra-Stability

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    Communication

    Vapochromic Behavior of a Chair-Shaped Supramolecular Metallacycle with Ultra-Stability
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    † †Shanghai Key Laboratory of Green Chemistry and Chemical Processes, School of Chemistry and Molecular Engineering, and ⊥Shanghai Key Laboratory of Magnetic Resonance, Department of Physics, East China Normal University, Shanghai 200062, P. R. China
    ‡ Department of Chemistry, Beijing Normal University, Beijing 100050, P. R. China
    § Department of Chemistry and Biochemistry, Texas State University, San Marcos, Texas 78666, United States
    *[email protected]
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    Cite this: J. Am. Chem. Soc. 2016, 138, 3, 738–741
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    https://doi.org/10.1021/jacs.5b11409
    Published January 7, 2016
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    Abstract

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    A new discrete supramolecular metallacycle functionalized with an alkynylplatinum(II) bzimpy moiety was successfully prepared via coordination-driven self-assembly, and it displayed a reversible color change in the solid state between yellow and red, triggered by CH2Cl2 vapor or mechanical grinding. Notably, unlike many known vapochromic systems, the obtained vapochromic metallacycle exhibits ultra-stability, with the red color remaining unchanged in air for several months at room temperature or even under vacuum for >1 week. Further investigation revealed that the chair conformation of the metallacyclic scaffold, which was thought to prevent intermolecular steric repulsion between the alkyl chain and triethylphosphine, favored close molecular stacking through intermolecular Pt···Pt and π–π stacking interactions, thus allowing such vapochromic behavior with ultra-stability.

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    Cite this: J. Am. Chem. Soc. 2016, 138, 3, 738–741
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