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Influence of Different Inorganic Salts on the Ionicity and Thermophysical Properties of 1-Ethyl-3-methylimidazolium Acetate Ionic Liquid
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    Influence of Different Inorganic Salts on the Ionicity and Thermophysical Properties of 1-Ethyl-3-methylimidazolium Acetate Ionic Liquid
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    Instituto de Tecnologia Química e Biológica António Xavier, Universidade Nova de Lisboa, Apartado 127, 2780-157 Oeiras, Portugal
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    Journal of Chemical & Engineering Data

    Cite this: J. Chem. Eng. Data 2015, 60, 3, 781–789
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    https://doi.org/10.1021/je5008857
    Published January 29, 2015
    Copyright © 2015 American Chemical Society

    Abstract

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    The ionicity of ionic liquids (IL) is related to the ionic nature of these fluids and is a useful indicator of the characteristic properties of a given ionic liquid. In this work, we studied the effects caused by the addition of different inorganic salts (IS), on the ionicity of the ionic liquid 1-ethyl-3-methylimidazolium acetate. The solubility of different inorganic salts, based on the ammonium and the sodium cations, in this IL at room temperature was experimentally determined. Thermophysical properties, such as viscosity, density, conductivity, and refractive indexes, of the 1-ethyl-3-methylimidazolium acetate + inorganic salt mixtures were measured in different concentrations of IS, and the ionicity of the systems was calculated. The results showed that when ammonium-based salts are used, the ionicity of the ionic liquid can be increased, leading to the formation of high ionicity ionic liquids.

    Copyright © 2015 American Chemical Society

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    Supporting Information

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    NMR and MS spectra of the synthesized salt ammonium ethanesulfonate as well as tables with all the experimental data for the density, viscosity, conductivity, refractive index, activation energy, molar volume, molar refraction, and free volume for all the IL + IS systems. The values for the theoretical molar volumes and molecular ionic radius for the IL and ISs used in this work are also presented. This material is available free of charge via the Internet at http://pubs.acs.org.

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    Cited By

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    This article is cited by 18 publications.

    1. Marta Królikowska, Nina Gos, Michał Skonieczny. Temperature and Composition Dependence of the Thermodynamic Properties of an Aqueous Solution of 1-Ethyl-3-methylimidazolium Formate and 1-Ethyl-3-methylimidazolium Acetate. Journal of Chemical & Engineering Data 2021, 66 (8) , 3300-3314. https://doi.org/10.1021/acs.jced.1c00349
    2. Kateryna Goloviznina, José N. Canongia Lopes, Margarida Costa Gomes, Agílio A. H. Pádua. Transferable, Polarizable Force Field for Ionic Liquids. Journal of Chemical Theory and Computation 2019, 15 (11) , 5858-5871. https://doi.org/10.1021/acs.jctc.9b00689
    3. Laura de Pablo Nisa, Muteng Mugang, María Dolores Bermejo, José Juan Segovia Puras, Eduardo Pérez. Density and Melting Points for the Binary Mixtures Dimethyl Sulfoxide (DMSO) + 1-Ethyl-3-methylimidazolium Acetate and DMSO + Choline Acetate. Journal of Chemical & Engineering Data 2019, 64 (7) , 2923-2928. https://doi.org/10.1021/acs.jced.8b01048
    4. Filipe S. Oliveira, Ralf Dohrn, Luís P. N. Rebelo, and Isabel M. Marrucho . Improving the Separation of n-Heptane + Ethanol Azeotropic Mixtures Combining Ionic Liquid 1-Ethyl-3-methylimidazolium Acetate with Different Inorganic Salts. Industrial & Engineering Chemistry Research 2016, 55 (20) , 5965-5972. https://doi.org/10.1021/acs.iecr.6b00810
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    13. Wenjun Chen, Jingyun Jiang, Xue Lan, Xinhui Zhao, Hongyu Mou, Tiancheng Mu. A strategy for the dissolution and separation of rare earth oxides by novel Brønsted acidic deep eutectic solvents. Green Chemistry 2019, 21 (17) , 4748-4756. https://doi.org/10.1039/C9GC00944B
    14. Fuxin Yang, Xiaopo Wang, Qiang Chen, Houzhang Tan. Improvement of the properties of 1-ethyl-3-methylimidazolium acetate using organic solvents for biofuel process. Journal of Molecular Liquids 2019, 284 , 82-91. https://doi.org/10.1016/j.molliq.2019.03.144
    15. Reza Haghbakhsh, Sona Raeissi. Estimation of viscosities of 1-alkyl-3-methylimidazolium ionic liquids over a range of temperatures using a simple correlation. Physics and Chemistry of Liquids 2019, 57 (3) , 401-421. https://doi.org/10.1080/00319104.2018.1480021
    16. Mercedes G. Montalbán, Mar Collado-González, A. Abel Lozano-Pérez, F. Guillermo Díaz Baños, Gloria Víllora. Extraction of organic compounds involved in the kinetic resolution of rac-2-pentanol from n-hexane by imidazolium-based ionic liquids: Liquid-liquid equilibrium. Journal of Molecular Liquids 2018, 252 , 445-453. https://doi.org/10.1016/j.molliq.2017.12.157
    17. Filipe S. Oliveira, Ralf Dohrn, Ana B. Pereiro, João M.M. Araújo, Luís P.N. Rebelo, Isabel M. Marrucho. Designing high ionicity ionic liquids based on 1-ethyl-3-methylimidazolium ethyl sulphate for effective azeotrope breaking. Fluid Phase Equilibria 2016, 419 , 57-66. https://doi.org/10.1016/j.fluid.2016.03.004
    18. Filipe S. Oliveira, Eurico J. Cabrita, Smilja Todorovic, Carlos E. S. Bernardes, José N. Canongia Lopes, Jennifer L. Hodgson, Douglas R. MacFarlane, Luís P. N. Rebelo, Isabel M. Marrucho. Mixtures of the 1-ethyl-3-methylimidazolium acetate ionic liquid with different inorganic salts: insights into their interactions. Physical Chemistry Chemical Physics 2016, 18 (4) , 2756-2766. https://doi.org/10.1039/C5CP06937H

    Journal of Chemical & Engineering Data

    Cite this: J. Chem. Eng. Data 2015, 60, 3, 781–789
    Click to copy citationCitation copied!
    https://doi.org/10.1021/je5008857
    Published January 29, 2015
    Copyright © 2015 American Chemical Society

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