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Binary Vapor–Liquid and Vapor–Liquid–Liquid Equilibria of Hydrofluorocarbons (HFC-125 and HFC-143a) and Hydrofluoroethers (HFE-125 and HFE-143a) with Ionic Liquid [emim][Tf2N]

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DuPont Central Research and Development, Experimental Station E304, Wilmington, Delaware 19880, and DuPont Fluoroproducts Laboratory, Chestnut Run Plaza 711, Wilmington, Delaware 19880
* Corresponding author. E-mail: [email protected]
†DuPont Central Research and Development.
‡DuPont Fluoroproducts Laboratory.
Cite this: J. Chem. Eng. Data 2008, 53, 2, 492–497
Publication Date (Web):December 30, 2007
https://doi.org/10.1021/je700588d
Copyright © 2008 American Chemical Society
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    Abstract

    Solubility behaviors of binary HFC-125 (CF3−CF2H), HFE-125 (CF3−O−CF2H), HFC-143a (CF3−CH3), and HFE-143a (CF3−O−CH3) systems with room-temperature ionic liquid 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide ([emim][Tf2N]) have been studied using a gravimetric microbalance method from (283 to 348) K and/or volumetric and cloud-point methods. Vapor–liquid equilibrium (VLE) data for HFC-125 + [emim][Tf2N] and HFE-125 + [emim][Tf2N] systems have been well correlated with our equation-of-state (EOS) model, which predicted vapor–liquid–liquid equilibria (VLLE) for both of these binary systems, and the VLLE have been experimentally proved. As for the binary systems of HFC-143a + [emim][Tf2N] and HFE-143a + [emim][Tf2N], only VLLE experiments have been made, and partial miscibility (temperature and composition: VLLE−Tx) data are well correlated with the NRTL (nonrandom two-liquids) activity model. While the immiscibility gap of the HFC-125 binary system is smaller than that of the HFE-125 system, the immiscibility behaviors for the HFC-143a and HFE-143a systems are opposite; the HFE-143a system is more soluble.

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