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Temperature Dependence of Solubility of Individual Light Fullerenes and Industrial Fullerene Mixture in 1-Chloronaphthalene and 1-Bromonaphthalene

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Saint Petersburg State University, Universitetskii pr. 26, St. Petersburg, Russia, 198504, and ILIP Ltd. (Innovations of Leningrad Universities and Enterprises), Instrumentalnaya ul. 6, St. Petersburg, Russia, 197022
* Corresponding author. Tel.: (812)3476435; fax: (812)2349859. E-mail address: [email protected] (K.N.S.).
†Saint-Petersburg State University.
‡ILIP Ltd. (Innovations of Leningrad Universities and Enterprises).
Cite this: J. Chem. Eng. Data 2010, 55, 7, 2373–2378
Publication Date (Web):March 31, 2010
https://doi.org/10.1021/je900814w
Copyright © 2010 American Chemical Society
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    Abstract

    The paper presents some data on the temperature dependence of solubility of individual light fullerenes (C60 and C70) and industrial fullerene mixtures (w1 = 0.65 C60 + w2 = 0.34 C70 + w3 = 0.01 Cn (n = 76 to 90)) in 1-chloronaphthalene and 1-bromonaphthalene in the temperature range from (10 to 60) °C. Solubility and density temperature dependences are presented and characterized; compositions of equilibrium solid phases are determined.

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    Optical spectra of fullerene solutions in 1-chloronaphthalene and 1-bromonaphthalene; the photos of solid solvates C70·1.5C10H7Cl and C70·1.5C10H7Br made on a polarizing microscope; temperature dependences of density of the C60 fullerene, C70 fullerene, and industrial fullerene mixture solutions in 1-chloronaphthalene and 1-bromonaphthalene in the temperature range from (10 to 60) °C. This material is available free of charge via the Internet at http://pubs.acs.org.

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    This article is cited by 21 publications.

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    2. Gregorio García, Mert Atilhan, and Santiago Aparicio . Theoretical Study on the Solvation of C60 Fullerene by Ionic Liquids. The Journal of Physical Chemistry B 2014, 118 (38) , 11330-11340. https://doi.org/10.1021/jp507146r
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    4. Nikolay O. Mchedlov-Petrossyan . Fullerenes in Liquid Media: An Unsettling Intrusion into the Solution Chemistry. Chemical Reviews 2013, 113 (7) , 5149-5193. https://doi.org/10.1021/cr3005026
    5. Konstantin N. Semenov, Nikolai A. Charykov, and Viktor N. Keskinov . Fullerenol Synthesis and Identification. Properties of the Fullerenol Water Solutions. Journal of Chemical & Engineering Data 2011, 56 (2) , 230-239. https://doi.org/10.1021/je100755v
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    12. Konstantin N. Semenov, Nikolai A. Charykov, Igor V. Murin, Yuriy V. Pukharenko. Physico-chemical properties of the fullerenol-70 water solutions. Journal of Molecular Liquids 2015, 202 , 1-8. https://doi.org/10.1016/j.molliq.2014.12.002
    13. T. Gangadhar, Vinod I. Bhoi, S. Kumar, C. N. Murthy. Supramolecular self-assembly and nanoencapsulation of [60]fullerene by bis-β-cyclodextrin. Journal of Inclusion Phenomena and Macrocyclic Chemistry 2014, 79 (1-2) , 215-223. https://doi.org/10.1007/s10847-013-0347-5
    14. Vitaly V. Chaban, Cleiton Maciel, Eudes Eterno Fileti. Does the Like Dissolves Like Rule Hold for Fullerene and Ionic Liquids?. Journal of Solution Chemistry 2014, 43 (6) , 1019-1031. https://doi.org/10.1007/s10953-014-0155-6
    15. K. N. Semenov, N. A. Charykov, V. A. Keskinov, D. G. Letenko, V. A. Nikitin, E. G. Gruzinskaya. Synthesis and identification of bromofullerenes C70Br8 and C70Br10 and their solubility in some aromatic solvents. Russian Journal of General Chemistry 2013, 83 (4) , 670-673. https://doi.org/10.1134/S1070363213040105
    16. K. N. Semenov, N. A. Charykov, V. A. Keskinov, D. G. Letenko, V. A. Nikitin. Synthesis of fullerenol-70-d by direct oxidation and its identification. Russian Journal of General Chemistry 2013, 83 (4) , 674-678. https://doi.org/10.1134/S1070363213040117
    17. D. G. Letenko, V. A. Nikitin, K. N. Semenov, N. A. Charykov, A. S. Ivanov. Conductivity of aqueous solutions of fullerol synthesized by direct oxidation. Russian Journal of Physical Chemistry A 2012, 86 (12) , 1808-1815. https://doi.org/10.1134/S003602441212014X
    18. K. N. Semenov, N. A. Charykov, D. G. Letenko, V. A. Nikitin, V. I. Namazbaev, V. A. Keskinov, Yu. V. Pukharenko. Synthesis and protection effect of fullerenol-d. II. Modification of water-soluble priming enamel with fullerenol-d. Protection of Metals and Physical Chemistry of Surfaces 2012, 48 (3) , 334-339. https://doi.org/10.1134/S2070205112030161
    19. L. V. Tsetkova, V. A. Keskinov, N. A. Charykov, N. I. Alekseev, E. G. Gruzinskaya, K. N. Semenov, V. N. Postnov, O. A. Krokhina. Extraction of fullerene mixture from fullerene soot with organic solvents. Russian Journal of General Chemistry 2011, 81 (5) , 920-926. https://doi.org/10.1134/S1070363211050136
    20. K. N. Semenov, D. G. Letenko, N. A. Charykov, V. A. Nikitin, M. Yu. Matuzenko, V. A. Keskinov, V. N. Postnov, A. A. Kopyrin. Solubility and some properties of aqueous solutions of fullerenol-d and composition of crystal hydrates. Russian Journal of Applied Chemistry 2011, 84 (1) , 44-49. https://doi.org/10.1134/S1070427211010071
    21. K. N. Semenov, N. A. Charykov, V. N. Postnov, O. A. Krokhina, E. G. Gruzinskaya. Isothermal solubility of individual light fullerenes in the homologous series of n-alkanes, n-alkanols, n-alkylcarboxylic acids, and arenes. Russian Journal of General Chemistry 2010, 80 (12) , 2443-2449. https://doi.org/10.1134/S1070363210120078
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