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Importance of the Nature of α-Substituents in Pyrrolidine Organocatalysts in Asymmetric Michael Additions
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    Importance of the Nature of α-Substituents in Pyrrolidine Organocatalysts in Asymmetric Michael Additions
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    Department of Chemistry, Indian Institute of Technology Bombay, Powai, Mumbai 400076, India
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    The Journal of Organic Chemistry

    Cite this: J. Org. Chem. 2010, 75, 21, 7310–7321
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    https://doi.org/10.1021/jo101592b
    Published October 14, 2010
    Copyright © 2010 American Chemical Society

    Abstract

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    The fundamental factors contributing toward the stereoselectivity in organocatalyzed asymmetric Michael reaction between aldehydes (propanal and 3-phenyl propanal) and methyl vinyl ketone (MVK) are established by using density functional theory methods. Three of the most commonly employed α-substituted pyrrolidine organocatalysts are examined. Several key stereochemical modes of addition between (i) a model enamine or (ii) pyrrolidine enamines derived from aldehydes and secondary amine to MVK are examined. Among these possibilities, the addition of (E)-enamine to cis-MVK is found to have a lower activation barrier. The stereochemical outcome of the reaction is reported on the basis of the relative energies between pertinent diastereomeric transition states. Moderate selectivity is predicted for the reaction involving pyrrolidine catalysts I and II, which carry relatively less bulky α-substituents dimethylmethoxymethyl and diphenylmethyl, respectively. On the other hand, high selectivity is computed in the case of catalyst III having a sufficiently large α-substituent (diarylmethoxymethyl or diphenylprolinol methyl ether). The enantiomeric excess in the case of 3-phenyl propanal is found to be much higher as compared to that with unsubstituted propanal, suggesting potential for improvement in stereoselectivity by substrate modifications. The computed enantiomeric excess is found to be in reasonable agreement with the reported experimental stereoselectivities. A detailed investigation on the geometries of the crucial transition states reveals that apart from steric interactions between the α-substituent and MVK, various other factors such as orbital interactions and weak stabilizing hydrogen-bonding interactions play a vital role in stereoselectivity. The results serve to establish the importance of cumulative effects of various stabilizing and destabilizing interactions at the transition state as responsible for the stereochemical outcome of the reaction. The limitations of commonly employed qualitative propositions, relying on the steric protection of one of the prochiral faces of enamines offered by the bulky α-substituent, are presented.

    Copyright © 2010 American Chemical Society

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    Supporting Information

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    Optimized geometries for all stationary points obtained at different levels of theory, total electronic energies, bond order, natural charges, AIM analyses, and IRC plots for transition states. This material is available free of charge via the Internet at http://pubs.acs.org.

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    The Journal of Organic Chemistry

    Cite this: J. Org. Chem. 2010, 75, 21, 7310–7321
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jo101592b
    Published October 14, 2010
    Copyright © 2010 American Chemical Society

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