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Parameters of the Protein Energy Landscapes of Several Light-Harvesting Complexes Probed via Spectral Hole Growth Kinetics Measurements
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    Parameters of the Protein Energy Landscapes of Several Light-Harvesting Complexes Probed via Spectral Hole Growth Kinetics Measurements
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    Department of Physics, Concordia University, 7141 Sherbrooke Street West, Montreal, Quebec, H4B 1R6 Canada
    MRC Laboratory of Molecular Biology, Cambridge, United Kingdom
    § Technical University of Berlin, Germany
    University of Applied Sciences, Berlin, Germany
    Estacion Experimental Aula Dei (CSIC), Avda. Montañana, 50059 Zaragoza, Spain
    # NREL, Golden, Colorado, United States
    Other Access OptionsSupporting Information (1)

    The Journal of Physical Chemistry B

    Cite this: J. Phys. Chem. B 2011, 115, 12, 2737–2747
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    https://doi.org/10.1021/jp108775y
    Published March 10, 2011
    Copyright © 2011 American Chemical Society

    Abstract

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    The parameters of barrier distributions on the protein energy landscape in the excited electronic state of the pigment/protein system have been determined by means of spectral hole burning for the lowest-energy pigments of CP43 core antenna complex and CP29 minor antenna complex of spinach Photosystem II (PS II) as well as of trimeric and monomeric LHCII complexes transiently associated with the pea Photosystem I (PS I) pool. All of these complexes exhibit sixty to several hundred times lower spectral hole burning yields as compared with molecular glassy solids previously probed by means of the hole growth kinetics measurements. Therefore, the entities (groups of atoms), which participate in conformational changes in protein, appear to be significantly larger and heavier than those in molecular glasses. No evidence of a small (∼1 cm−1) spectral shift tier of the spectral diffusion dynamics has been observed. Therefore, our data most likely reflect the true barrier distributions of the intact protein and not those related to the interface or surrounding host. Possible applications of the barrier distributions as well as the assignments of low-energy states of CP29 and LHCII are discussed in light of the above results.

    Copyright © 2011 American Chemical Society

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    Supporting Information

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    Procedure for the fitting of absorption and (asymmetric) HB action spectra of CP29, LHCII monomer, and LHCII trimer. This material is available free of charge via the Internet at http://pubs.acs.org.

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    Cited By

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    This article is cited by 16 publications.

    1. Jörg Pieper, Petrica Artene, Margus Rätsep, Mihkel Pajusalu, Arvi Freiberg. Evaluation of Electron–Phonon Coupling and Spectral Densities of Pigment–Protein Complexes by Line-Narrowed Optical Spectroscopy. The Journal of Physical Chemistry B 2018, 122 (40) , 9289-9301. https://doi.org/10.1021/acs.jpcb.8b05220
    2. Mahboobe Jassas, Jinhai Chen, Anton Khmelnitskiy, Anna Paola Casazza, Stefano Santabarbara, Ryszard Jankowiak. Structure-Based Exciton Hamiltonian and Dynamics for the Reconstituted Wild-type CP29 Protein Antenna Complex of the Photosystem II. The Journal of Physical Chemistry B 2018, 122 (17) , 4611-4624. https://doi.org/10.1021/acs.jpcb.8b00032
    3. Adam Kell, Mahboobe Jassas, Kirsty Hacking, Richard J. Cogdell, and Ryszard Jankowiak . On Light-Induced Photoconversion of B800 Bacteriochlorophylls in the LH2 Antenna of the Purple Sulfur Bacterium Allochromatium vinosum. The Journal of Physical Chemistry B 2017, 121 (43) , 9999-10006. https://doi.org/10.1021/acs.jpcb.7b06185
    4. Nicoleta Herascu, Mark S. Hunter, Golia Shafiei, Mehdi Najafi, T. Wade Johnson, Petra Fromme, and Valter Zazubovich . Spectral Hole Burning in Cyanobacterial Photosystem I with P700 in Oxidized and Neutral States. The Journal of Physical Chemistry B 2016, 120 (40) , 10483-10495. https://doi.org/10.1021/acs.jpcb.6b07803
    5. Mehdi Najafi and Valter Zazubovich . Monte Carlo Modeling of Spectral Diffusion Employing Multiwell Protein Energy Landscapes: Application to Pigment–Protein Complexes Involved in Photosynthesis. The Journal of Physical Chemistry B 2015, 119 (25) , 7911-7921. https://doi.org/10.1021/acs.jpcb.5b02764
    6. Mehdi Najafi, Nicoleta Herascu, Golia Shafiei, Rafael Picorel, and Valter Zazubovich . Conformational Changes in Pigment–Protein Complexes at Low Temperatures—Spectral Memory and a Possibility of Cooperative Effects. The Journal of Physical Chemistry B 2015, 119 (23) , 6930-6940. https://doi.org/10.1021/acs.jpcb.5b02845
    7. Sepideh Skandary, Martin Hussels, Alexander Konrad, Thomas Renger, Frank Müh, Martin Bommer, Athina Zouni, Alfred J. Meixner, and Marc Brecht . Variation of Exciton-Vibrational Coupling in Photosystem II Core Complexes from Thermosynechococcus elongatus As Revealed by Single-Molecule Spectroscopy. The Journal of Physical Chemistry B 2015, 119 (11) , 4203-4210. https://doi.org/10.1021/jp510631x
    8. Valter Zazubovich . Fluorescence Line Narrowing and Δ-FLN Spectra in the Presence of Excitation Energy Transfer between Weakly Coupled Chromophores. The Journal of Physical Chemistry B 2014, 118 (47) , 13535-13543. https://doi.org/10.1021/jp509056z
    9. Nicoleta Herascu, Adam Kell, Khem Acharya, Ryszard Jankowiak, Robert E. Blankenship, and Valter Zazubovich . Modeling of Various Optical Spectra in the Presence of Slow Excitation Energy Transfer in Dimers and Trimers with Weak Interpigment Coupling: FMO as an Example. The Journal of Physical Chemistry B 2014, 118 (8) , 2032-2040. https://doi.org/10.1021/jp410586f
    10. Mehdi Najafi, Nicoleta Herascu, Michael Seibert, Rafael Picorel, Ryszard Jankowiak, and Valter Zazubovich . Spectral Hole Burning, Recovery, and Thermocycling in Chlorophyll–Protein Complexes: Distributions of Barriers on the Protein Energy Landscape. The Journal of Physical Chemistry B 2012, 116 (38) , 11780-11790. https://doi.org/10.1021/jp308055r
    11. Ryszard Jankowiak . Probing Electron-Transfer Times in Photosynthetic Reaction Centers by Hole-Burning Spectroscopy. The Journal of Physical Chemistry Letters 2012, 3 (12) , 1684-1694. https://doi.org/10.1021/jz300505r
    12. Nicoleta Herascu, Somaya Ahmouda, Rafael Picorel, Michael Seibert, Ryszard Jankowiak, and Valter Zazubovich . Effects of the Distributions of Energy or Charge Transfer Rates on Spectral Hole Burning in Pigment–Protein Complexes at Low Temperatures. The Journal of Physical Chemistry B 2011, 115 (50) , 15098-15109. https://doi.org/10.1021/jp208142k
    13. Ximao Feng, Bhanu Neupane, Khem Acharya, Valter Zazubovich, Rafael Picorel, Michael Seibert, and Ryszard Jankowiak . Spectroscopic Study of the CP43′ Complex and the PSI–CP43′ Supercomplex of the Cyanobacterium Synechocystis PCC 6803. The Journal of Physical Chemistry B 2011, 115 (45) , 13339-13349. https://doi.org/10.1021/jp206054b
    14. Ryszard Jankowiak, Mike Reppert, Valter Zazubovich, Jörg Pieper, and Tonu Reinot . Site Selective and Single Complex Laser-Based Spectroscopies: A Window on Excited State Electronic Structure, Excitation Energy Transfer, and Electron–Phonon Coupling of Selected Photosynthetic Complexes. Chemical Reviews 2011, 111 (8) , 4546-4598. https://doi.org/10.1021/cr100234j
    15. Valter Zazubovich, Ryszard Jankowiak. Biophotonics of Photosynthesis. 2015, 129-164. https://doi.org/10.1002/9781119011804.ch4
    16. Carolin König, Johannes Neugebauer. Quantum Chemical Description of Absorption Properties and Excited‐State Processes in Photosynthetic Systems. ChemPhysChem 2012, 13 (2) , 386-425. https://doi.org/10.1002/cphc.201100408

    The Journal of Physical Chemistry B

    Cite this: J. Phys. Chem. B 2011, 115, 12, 2737–2747
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jp108775y
    Published March 10, 2011
    Copyright © 2011 American Chemical Society

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