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    Molar Extinction Coefficient of Single-Wall Carbon Nanotubes
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    † Institute of Physical and Theoretical Chemistry, Department of Chemistry and Pharmacy, Julius-Maximilians University of Würzburg, D-97074 Würzburg, Germany
    ‡ Department of Engineering, University of Cambridge, Cambridge, CB3 OFA, U.K.
    E-mail: [email protected]
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    The Journal of Physical Chemistry C

    Cite this: J. Phys. Chem. C 2011, 115, 30, 14682–14686
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    https://doi.org/10.1021/jp205289h
    Published June 22, 2011
    Copyright © 2011 American Chemical Society
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    Abstract

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    The molar extinction coefficient of single-wall carbon nanotubes (SWNTs) is determined using fluorescence tagging, as well as atomic force microscopy (AFM) imaging, which facilitate the correlation of nanotube concentrations with absorption spectra. Tagging of SWNTs is achieved using fluorescence-labeled single-strand DNA oligomers as the dispersion additive, while AFM imaging is used to determine the mass of SWNTs in the retentate of vacuum-filtered colloidal SWNT suspensions. The resulting absorption cross section for the first exciton transition of (6,5) nanotubes of 1.7 × 10–17 cm2 per C-atom corresponds to an extinction coefficient of (4400 ± 1000) M–1·cm–1, which is equivalent to an oscillator strength of 0.010 per carbon atom.

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    Absorption spectra of DGU enriched DNA-FAM-SWNT samples; geometrical considerations for determination of the length of a SWNT segment covered by a single-strand DNA oligomer; DNA coverage; optical absorption and absorption cross section; vacuum filtration; and AFM characterization. This material is available free of charge via the Internet at http://pubs.acs.org.

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    Cite this: J. Phys. Chem. C 2011, 115, 30, 14682–14686
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    https://doi.org/10.1021/jp205289h
    Published June 22, 2011
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