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    One-Step Synthesis of Au–Pd Alloy Nanodendrites and Their Catalytic Activity
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    † State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, P. R. China
    ‡ University of Chinese Academy of Sciences, Beijing, 100049, P. R. China
    § Catalysis and Materials Division, Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, P. R. China
    ∥ Dalian National Laboratory for Clean Energy, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, P. R. China
    *Tel +86 411 84379015; Fax +86 411 84691570; e-mail [email protected] (T.Z.).
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    The Journal of Physical Chemistry C

    Cite this: J. Phys. Chem. C 2013, 117, 24, 12526–12536
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    https://doi.org/10.1021/jp4013202
    Published May 30, 2013
    Copyright © 2013 American Chemical Society
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    Abstract

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    Au–Pd bimetallic nanocrystals with well-defined dendritic morphology, uniform size, and homogeneous alloy structure were synthesized in an aqueous solution by using ascorbic acid as the reductant and triblock copolymer P123 as the stabilizing agent. In this synthesis, ascorbic acid played a key role in directing the nanodendritic morphology while the presence of Pd was mandatory for the formation of well-defined nanodendrites. Without Pd, only faceted nanoparticles of gold were formed under the same reaction conditions. Other reaction variables such as the addition sequence and the dropping rate of the metal precursors, the type and concentration of the stabilizing agents, and the reaction time and temperature were all found to affect the size uniformity and morphology perfectness to some extent. The Au/Pd atomic ratio could be tuned in a wide range without deteriorating the nanodendritic morphology. The as-prepared Au–Pd nanodendrites exhibited excellent catalytic activities toward electroxidation of methanol and reduction of 2-nitrophenol, and the catalytic performances could be effectively tuned by the Au/Pd ratio.

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    Scheme of the synthesis procedure, the TEM images, XRD patterns, UV–vis spectra, XPS spectra of the Au–Pd nanodendrites, and the activity per mass of catalyst for the reduction of 2-nitrophenol over Au–Pd nanodendrites. This material is available free of charge via the Internet at http://pubs.acs.org.

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    Cite this: J. Phys. Chem. C 2013, 117, 24, 12526–12536
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