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Influence of Surface Topography on the Interactions between Nanostructured Hydrophobic Surfaces

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YKI, Ytkemiska Institutet AB/Institute for Surface Chemistry, Box 5607, SE-114 86 Stockholm, Sweden
Department of Chemistry, Surface and Corrosion Science, KTH Royal Institute of Technology, SE-100 44 Stockholm, Sweden
§ Omya Development AG, CH-4665 Oftringen, Switzerland
School of Chemical Technology, Department of Forest Products Technology, Aalto University, P.O. Box 16300, FI-00076 Aalto, Finland
*Telephone: + 46 8 790 9920. Fax: +46 8 208 284. E-mail: [email protected]
Cite this: Langmuir 2012, 28, 21, 8026–8034
Publication Date (Web):May 3, 2012
https://doi.org/10.1021/la300628m
Copyright © 2012 American Chemical Society
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Abstract

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Nanostructured particle coated surfaces, with hydrophobized particles arranged in close to hexagonal order and of specific diameters ranging from 30 nm up to 800 nm, were prepared by Langmuir–Blodgett deposition followed by silanization. These surfaces have been used to study interactions between hydrophobic surfaces and a hydrophobic probe using the AFM colloidal probe technique. The different particle coated surfaces exhibit similar water contact angles, independent of particle size, which facilitates studies of how the roughness length scale affects capillary forces (previously often referred to as “hydrophobic interactions”) in aqueous solutions. For surfaces with smaller particles (diameter < 200 nm), an increase in roughness length scale is accompanied by a decrease in adhesion force and bubble rupture distance. It is suggested that this is caused by energy barriers that prevent the motion of the three-phase (vapor/liquid/solid) line over the surface features, which counteracts capillary growth. Some of the measured force curves display extremely long-range interaction behavior with rupture distances of several micrometers and capillary growth with an increase in volume during retraction. This is thought to be a consequence of nanobubbles resting on top of the surface features and an influx of air from the crevices between the particles on the surface.

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