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Boron Nitride Porous Microbelts for Hydrogen Storage

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† World Premier International Center for Materials Nanoarchitectonics (WPI-MANA), National Institute for Materials Science (NIMS), Namiki 1-1, Tsukuba, Ibaraki 305-0044, Japan
‡ Graduate School of Pure and Applied Sciences, University of Tsukuba, Tennodai 1, Tsukuba, Ibaraki 305-0005, Japan
§ Department of Physics and Materials Science, City University of Hong Kong, Tat Chee Avenue, Kowloon, Hong Kong
*Address correspondence to [email protected], [email protected], [email protected]
Cite this: ACS Nano 2013, 7, 2, 1558–1565
Publication Date (Web):January 9, 2013
https://doi.org/10.1021/nn305320v
Copyright © 2013 American Chemical Society
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Layered boron nitrides (BNs) are usually viewed as excellent protective coatings and reinforcing materials due to their chemical inertness and high mechanical strength. However, the attention paid to their potential applications in gas sorption, especially in case of hydrogen, has obviously been insufficient. Herein, a novel BN material (i.e., porous microbelts), with the highest specific surface area ever reported for any BN system, up to 1488 m2 g–1, is obtained through one-step template-free reaction of a boron acid–melamine precursor with ammonia. Comprehensive high-resolution transmission electron microscopy, X-ray diffraction, and Raman characterizations all confirm that the obtained BN phase is partially disordered, shows an enlarged average spacing between adjacent (0002) layers (d0002 = 0.38 nm, compared to normal 0.33 nm for a bulk layered BN), and belongs to an intermediate state between hexagonal (h-BN) and amorphous (a-BN) phases. By changing the synthesis temperatures, the textures of obtained porous microbelts are adjustable. H2 sorption evaluations demonstrate that the materials exhibit high and reversible H2 uptake from 1.6 to 2.3 wt % at 77 K and at a relatively low pressure of 1 MPa.

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Structures of BN microrods, loosened belt bundles, and isolated belts; morphology of BNPB-900 and BNPB-1000 samples; list of Raman shifts for all samples; evolution of XRD, Raman spectra, and HRTEM of BNPB-1100 after annealing at 1500 °C; chemical compositions of BNPB-900 and BNPB-1000 samples; P/P0 range selections and seven-point linear simulation of BET equiation; textural characteristics and hydrogen uptake summary table of all products. This material is available free of charge via the Internet at http://pubs.acs.org.

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