Isolation and Structural Characterization of a Lewis Base-Free Monolithioferrocene
Abstract

A sterically hindered ferrocenyl lithium derivative was successfully isolated as a stable, crystalline compound without any stabilization by Lewis bases. On the grounds of X-ray crystallography and multinuclear NMR spectroscopy, a dimeric structure was assigned to this monolithioferrocene in the crystalline state and in solution.
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